The influence of the structure on the electrical and magnetic properties of Bi2Sr2CaCu2O8+delta single crystals

被引:4
作者
Aldica, G [1 ]
Crisan, A [1 ]
VelterStefanescu, M [1 ]
Mandache, S [1 ]
Bunescu, MC [1 ]
机构
[1] METAV SA,BUCHAREST,ROMANIA
关键词
D O I
10.1023/A:1018579817471
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
The correlation between the structure, chemical composition, electrical and magnetic properties of Bi2Sr2CaCu2O8+delta single crystals is presented. As revealed by SEM measurements, the small samples (approximately 1 mm x 1 mm x 0.2 mm) are stacks of thin plates (1-2 mu m). Microcompositional measurements (energy dispersive spectroscopy) show the Bi2Sr2CaCu2O8+delta (2212)-phase and a small quantity of residual phases enriched in bismuth and strontium and calcium-deficient. Magnetically modulated microwave absorption measurements (MAMMA) lead to a value for the anisotropy of the upper critical field of about 7, which is more than twice the reported value for YBa2Cu3O7-delta single crystals (also determined from MAMMA responses). The plot of the resistance versus temperature suggests that only the first 10-20 plates from the surface of the sample have a contribution to the sample conductivity. The imaginary part, chi'', of the magnetic susceptibility of our samples shows three peaks.
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页码:1195 / 1199
页数:5
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