Effect of Pre-treatment and Calcination Process on Micro-Structural and Physico-Chemical Properties of Hydroxyapatite derived from Chicken Bone Bio-waste

被引:21
作者
Barua, Emon [1 ]
Deoghare, Ashish B. [1 ]
Deb, Payel [1 ]
Das Lala, Sumit [1 ]
Chatterjee, Sushovan [2 ]
机构
[1] Natl Inst Technol Silchar, Dept Mech Engn, Silchar 788010, Assam, India
[2] Cooch Behar Govt Engn Coll, Dept Mech Engn, Cooch Behar 736170, W Bengal, India
关键词
Hydroxyapatite; Chicken bone bio-waste; Biomaterial; Bone tissue engineering; Calcination; NANOCRYSTALLINE HYDROXYAPATITE; FISH SCALE;
D O I
10.1016/j.matpr.2019.04.191
中图分类号
T [工业技术];
学科分类号
120111 [工业工程];
摘要
This study reports the feasibility of isolation of hydroxyapatite (HA) from chicken bone bio-waste and the effect of pre-treatment and calcination process of bones on micro-structural and physico-chemical properties of HA. Chicken bones are treated with acid, alkali and acid-alkali solution followed by calcination at 700, 800 and 900 degrees C respectively. The calcined bones are characterized and compared. It is found that acid treated bones calcined at 900 degrees C yields pure phase of crystalline HA particles of size 600 nm with good pore morphology having pore diameter 208 nm, Ca/P atomic ratio of 1.653 and high thermal stability, ideal for biomedical applications. (C) 2019 Elsevier Ltd. All rights reserved.
引用
收藏
页码:188 / 198
页数:11
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