Synthesis and solid state structural analysis of 1,3-alternate conformer of tetrathiacalix[4]arene tetra-ester, -acid and -ether derivatives

被引:39
作者
Akdas, H
Jaunky, W
Graf, E
Hosseini, MW
Planeix, JM
De Cian, A
Fischer, J
机构
[1] Univ Strasbourg 1, CNRS, Chim Coordinat Organ Lab, Inst Le Bel, F-67000 Strasbourg, France
[2] Univ Strasbourg 1, CNRS, Lab Cristallochim & Chim Subst, Inst Le Bel, F-67000 Strasbourg, France
关键词
D O I
10.1016/S0040-4039(00)00453-6
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Four new tetrathiacalix[4]arene derivatives blocked in 1,3-alternate conformation and bearing four ester, acid or ether groups were prepared and their 1,3-alternate conformation was established by X-ray diffraction methods on single-crystal. (C) 2000 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:3601 / 3606
页数:6
相关论文
共 23 条
  • [1] Thiacalixarenes:: Synthesis and structural analysis of thiacalix[4]arene and of p-tert-butylthiacalix[4]arene
    Akdas, H
    Bringel, L
    Graf, E
    Hosseini, MW
    Mislin, G
    Pansanel, J
    De Cian, A
    Fischer, J
    [J]. TETRAHEDRON LETTERS, 1998, 39 (16) : 2311 - 2314
  • [2] Synthesis and solid state structural analysis of conformers of tetrakis((ethoxycarbonyl)methoxy)tetrathiacalix[4]arene
    Akdas, H
    Mislin, G
    Graf, E
    Hosseini, MW
    De Cian, A
    Fischer, J
    [J]. TETRAHEDRON LETTERS, 1999, 40 (11) : 2113 - 2116
  • [3] BILYK A, 2000, IN PRESS EUR J INORG
  • [4] DELAIGUE X, 1995, CHEM COMMUN, P609
  • [5] DELAIGUE X, 1994, CHEM COMMUN, P1579
  • [6] CALIXARENES .31. SYNTHESIS AND CONFORMATION OF P-TERT-BUTYLTETRAMERCAPTOCALIX[4]ARENE
    GIBBS, CG
    GUTSCHE, CD
    [J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1993, 115 (12) : 5338 - 5339
  • [7] Gutsche C. D, 1998, MONOGRAPHS SUPRAMOLE
  • [8] Crystal engineering: molecular networks based on inclusion phenomena
    Hosseini, MW
    De Cian, A
    [J]. CHEMICAL COMMUNICATIONS, 1998, (07) : 727 - 733
  • [9] Selective synthesis of three conformational isomers of tetrakis[(ethoxycarbonyl)methoxy]thiacalix[4]arene and their complexation properties towards alkali metal ions
    Iki, N
    Narumi, F
    Fujimoto, T
    Morohashi, N
    Miyano, S
    [J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 2, 1998, (12): : 2745 - 2750
  • [10] Selective oxidation of thiacalix[4]arenes to the sulfinyl- and sulfonylcalix[4]arenes and their coordination ability to metal ions
    Iki, N
    Kumagai, H
    Morohashi, N
    Ejima, K
    Hasegawa, M
    Miyanari, S
    Miyano, S
    [J]. TETRAHEDRON LETTERS, 1998, 39 (41) : 7559 - 7562