Currents on ultrasound-assisted extraction for sample preparation and spectroscopic analytes determination

被引:64
作者
Júnior, DS
Krug, FJ
Pereira, MD
Korn, M
机构
[1] Univ Estado da Bahia, Dept Ciencias Exatas & Terra, BR-41195001 Salvador, BA, Brazil
[2] Univ Sao Paulo, Ctr Energia Nucl Agr, Piracicaba, SP, Brazil
关键词
sample preparation; ultrasound-assisted extraction; spectroscopic techniques;
D O I
10.1080/05704920600620436
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 [仪器科学与技术]; 080401 [精密仪器及机械]; 081102 [检测技术与自动化装置];
摘要
This review reports recent applications of the ultrasonic energy for extracting inorganic and organic analytes from diverse solid samples devoted to spectroscopic analyses. The main advantages resulting from ultrasound comprise the reduction of the procedural time and reagent consumption. In this sense, ultrasound-assisted extractions can be considered as an efficient tool for improving the analytical performance of procedures employed in analytical chemistry and natural products chemistry. However, a rigorous experimental control is strongly recommended in order to avoid losses in precision and accuracy. Uncontrolled ultrasound-assisted extraction procedure is also discussed, since ultrasonic irradiation can provoke decompositions of molecules, hindering organic compounds extraction.
引用
收藏
页码:305 / 321
页数:17
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