Structural and magnetic characterization of self-assembled iron oxide nanoparticle arrays

被引：38

作者：

Benitez, M. J. ^{[1
,2
]}

Mishra, D. ^{[1
]}

Szary, P. ^{[1
]}

Confalonieri, G. A. Badini ^{[1
]}

Feyen, M. ^{[2
]}

Lu, A. H. ^{[2
]}

Agudo, L. ^{[3
]}

Eggeler, G. ^{[3
]}

Petracic, O. ^{[1
]}

Zabel, H. ^{[1
]}

机构：

[1] Ruhr Univ Bochum, Inst Expt Phys Festkorperphys, D-44780 Bochum, Germany

[2] Max Planck Inst Kohlenforsch, D-45470 Mulheim An Der Ruhr, Germany

[3] Ruhr Univ Bochum, Inst Werkstoffe, D-44780 Bochum, Germany

来源：

JOURNAL OF PHYSICS-CONDENSED MATTER | 2011年 / 23卷 / 12期

关键词：

EXCHANGE BIAS; VERWEY TRANSITION; FE3O4; NANOCRYSTALS; BEHAVIOR; SIZE;

D O I：

10.1088/0953-8984/23/12/126003

中图分类号：

O469 [凝聚态物理学];

学科分类号：

070205 [凝聚态物理];

摘要：

We report about a combined structural and magnetometric characterization of self-assembled magnetic nanoparticle arrays. Monodisperse iron oxide nanoparticles with a diameter of 20 nm were synthesized by thermal decomposition. The nanoparticle suspension was spin-coated on Si substrates to achieve self-organized arrays of particles and subsequently annealed at various conditions. The samples were characterized by x-ray diffraction, and bright and dark field high resolution transmission electron microscopy. The structural analysis is compared to magnetization measurements obtained by superconducting quantum interference device magnetometry. We can identify either multi-phase FexO/gamma-Fe2O3 or multi-phase FexO/Fe3O4 nanoparticles. The FexO/gamma-Fe2O3 system shows a pronounced exchange bias effect which explains the peculiar magnetization data found for this system.

引用

页数：12

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