Efficient solvent-free O-silylation of alcohols with R3SiCl

被引:22
作者
Hatano, B [1 ]
Toyota, S [1 ]
Toda, F [1 ]
机构
[1] Okayama Univ Sci, Fac Sci, Dept Chem, Okayama 7000005, Japan
关键词
D O I
10.1039/b102447g
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Solvent-free O-silylation of liquid or crystalline alcohols with liquid or crystalline silyl chlorides proceeds efficiently to give silyl ethers in good yield. O-Silylation of sterically hindered alcohols which cannot be performed in solution is also accomplished efficiently under solvent-free conditions.
引用
收藏
页码:140 / 142
页数:3
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