Synthesis and X-ray characterization of Li(1-2x)NixTiO(PO4) (0≤x≤0.50)

被引：2

作者：

Manoun, B

El Jazouli, A

Gravereau, P

Chaminade, JP

机构：

[1] Fac Sci, Lab Chim Mat Solides, Casablanca, Morocco

[2] Inst Chim Mat Condensee Bordeaux, F-33608 Pessac, France

来源：

POWDER DIFFRACTION | 2003年 / 18卷 / 04期

关键词：

oxyphosphates; X-ray diffraction; Li(1-2x)NixTiO(PO4);

D O I：

10.1154/1.1596631

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

Li(1 - 2x)NixTiO(PO4) oxyphosphate powders were prepared from dilute solutions of NiCl2.6 H2O, Li2CO3, (NH4)(2)HPO4, and TiCl4 in ethanol. The final temperature was 850degreesC. Li(1 - 2x)NixTiO(PO4) oxyphosphates with 0 less than or equal to x less than or equal to 0.10 crystallize in the orthorhombic system with space group Pnma, while those with 0.10 < x less than or equal to 0.25 crystallize in the monoclinic system with space group P2(1)/c. (C) 2003 International Centre for Diffraction Data.

引用

页码：301 / 305

页数：5

共 8 条

[1] INDEXING OF POWDER DIFFRACTION PATTERNS FOR LOW-SYMMETRY LATTICES BY THE SUCCESSIVE DICHOTOMY METHOD [J].