Impact of ultrasonic energy on the crystallization of dextrose monohydrate

被引:27
作者
Devarakonda, S
Evans, JMB
Myerson, AS [1 ]
机构
[1] IIT, Dept Chem Engn, Chicago, IL 60616 USA
[2] Polytech Univ, Dept Chem Engn, Metrotech Ctr 6, Brooklyn, NY 11201 USA
关键词
D O I
10.1021/cg034056r
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
In this paper, we investigate the potential of ultrasonic energy in assisting the crystallization of dextrose monohydrate, which is primarily manufactured via slow cool batch, lasting 48 h (0.5 degreesC/h), seeded crystallization; this cooling curve is designed to optimize the crystal growth and give rise to relatively large dextrose crystals. This study was interested in the impact of ultrasound on the nucleation, crystal breakage/size distribution, and rate of growth of the dextrose, while producing a product of the desired crystal size distribution. Experimental results show that ultrasonic energy can be used to induce nucleation and increase the overall mass rate of crystal growth while producing product with the desired crystal size distribution.
引用
收藏
页码:741 / 746
页数:6
相关论文
共 11 条
[1]   Crystallization of potash alum: effect of power ultrasound [J].
Amara, N ;
Ratsimba, B ;
Wilhelm, AM ;
Delmas, H .
ULTRASONICS SONOCHEMISTRY, 2001, 8 (03) :265-270
[2]   Density and refractive index for boric acid plus potassium chloride plus water and disodium tetraborate plus potassium chloride plus water systems at (20, 25, and 30) °C [J].
Galleguillos, HR ;
Flores, EK ;
Aguirre, CE .
JOURNAL OF CHEMICAL AND ENGINEERING DATA, 2001, 46 (06) :1632-1634
[3]   Comparison of the effects of ultrasound and mechanical agitation on a reacting solid-liquid system [J].
Hagenson, LC ;
Doraiswamy, LK .
CHEMICAL ENGINEERING SCIENCE, 1998, 53 (01) :131-148
[4]  
*LAS SENS TECHN IN, 1998, LAS M100 HARDW MAN
[5]   Rapid sonocrystallization in the salting-out process [J].
Li, H ;
Wang, JK ;
Bao, Y ;
Guo, ZC ;
Zhang, MY .
JOURNAL OF CRYSTAL GROWTH, 2003, 247 (1-2) :192-198
[6]  
McCausland LJ, 2001, CHEM ENG PROG, V97, P56
[7]  
MULLIN JW, 1997, CRYSTALLIZATION, P172
[8]  
Myerson A. S., 2002, HDB IND CRYSTALLIZAT, P43
[9]  
ROZENBERG LD, 1973, PHYSICAL PRINCIPLES
[10]   SONOCHEMISTRY [J].
SUSLICK, KS .
SCIENCE, 1990, 247 (4949) :1439-1445