Studies of Fe-doped SiO2/TiO2 composite nanoparticles prepared by sol-gel-hydrothermal method

被引:28
作者
Li, ZJ
Hou, B
Xu, Y
Wu, D
Sun, YH [1 ]
机构
[1] Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Convers, Taiyuan 030001, Peoples R China
[2] Chinese Acad Sci, Grad Sch, Beijing 100039, Peoples R China
基金
中国国家自然科学基金;
关键词
D O I
10.1007/s10853-005-0521-2
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Fe-doped SiO2/TiO2 composite nanoparticles were directly prepared by sol-gel-hydrothermal process, and characterized by X-ray diffraction (XRD), transmission electron microscope (TEM), thermal gravimetry (TG), X-Ray photoelectron spectroscopy (XPS), and UV-Vis diffuse reflectance spectra (DRS). It was found that the Fe3+ was well dispersed in solid solution Of SiO2/TiO2 composite nanoparticles that was about 10 nm with spherical morphology and rich silica layer external surface. It could effectively offer broadband shield for both UVB (290-320 nm) and UVA (320-400 nm). The results of Photodecomposition of methylene blue showed that the photoactivity of Fe-doped SiO2/TiO2 composite was minimized due to the addition of iron ion. (c) 2005 Springer Science + Business Media, Inc.
引用
收藏
页码:3939 / 3943
页数:5
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