Biopolymer-assisted green synthesis of iron oxide nanoparticles and their magnetic properties

被引:82
作者
Gao, Shuyan [1 ]
Shi, Youguo [2 ]
Zhang, Shuxia [1 ]
Jiang, Kai [1 ]
Yang, Shuxia [1 ]
Li, Zhengdao [1 ]
Takayama-Muromachi, Eiji [2 ]
机构
[1] Henan Normal Univ, Coll Chem & Environm Sci, Xinxiang 453007, Peoples R China
[2] Natl Inst Mat Sci, ANML, Tsukuba, Ibaraki 3050044, Japan
关键词
D O I
10.1021/jp802500a
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Magnetite nanoparticles were fabricated using a biopolymer (sodium alginate)-assisted route via redox-based hydrothermal method using FeCl3 center dot 6H(2)O and urea as the starting materials. The morphology, composition, and phase structure of as-prepared powders were characterized by scanning electron microscopy (SEM), X-ray diffraction (XRD), and X-ray photoelectron spectroscopy (XPS). The results show that biopolymer plays dual roles, reduction, and stabilization, in the formation of the products. This method can be easily controlled and is expected to be applicable for the preparation of other metal oxides. The sample demonstrated a typical ferromagnetic behavior from a direct current SQUID magnetometer (Quantum Design MPMS).
引用
收藏
页码:10398 / 10401
页数:4
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