Automated solid-phase extraction for sample preparation followed by high-performance liquid chromatography with diode array and mass spectrometric detection for the analysis of resveratrol derivatives in wine

被引：67

作者：

Domínguez, C ^{[1
]}

Guillén, DA ^{[1
]}

Barroso, CG ^{[1
]}

机构：

[1] Univ Cadiz, Fac Ciencias, Dept Quim Analit, E-11510 Puerto Real, Cadiz, Spain

来源：

JOURNAL OF CHROMATOGRAPHY A | 2001年 / 918卷 / 02期

关键词：

sample preparation; wine; food analysis; resveratrol; glycosides; phenolic compounds;

D O I：

10.1016/S0021-9673(01)00748-8

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A method has been developed for the simultaneous determination of resveratrol in all its forms. (free isomers and glycosylates) in wines by high-performance liquid chromatography with diode array and mass spectrometric detection. Prior to injection into the column, preconcentration of the sample by automated solid-phase extraction is carried out. In the detection by UV absorption, quantitation was carried out at 280 and 305 nm, and in detection by mass spectrometry, quantitation was performed in the selected ion monitoring mode at m/z 228 and at m/z 238. A comparative study between both detection systems was carried out. (C) 2001 Elsevier Science B.V. All rights reserved.

引用

页码：303 / 310

页数：8

共 37 条

[1] Techniques for resveratrol silylation [J].

Antonelli, A ;

Fabbri, C ;

Lercker, G .

CHROMATOGRAPHIA, 1996, 42 (7-8) :469-472

[2]

BESSIS R, 1997, REV OENOLOGUES, V85, P5

[3]

BLOND JP, 1995, SCI ALIMENT, V15, P347

[4]

Bravo-Abad F., 1996, Alimentaria, P71

[5]

Brun S., 1995, Cahiers de Nutrition et de Dietetique, V30, P224

[6] RESVERATROL PRODUCTION AS A PART OF THE HYPERSENSITIVE-LIKE RESPONSE OF GRAPEVINE CELLS TO AN ELICITOR FROM TRICHODERMA-VIRIDE [J].

CALDERON, AA ;

ZAPATA, JM ;

MUNOZ, R ;

PEDRENO, MA ;

BARCELO, AR .

NEW PHYTOLOGIST, 1993, 124 (03) :455-463

[7] Resveratrol content of some wines obtained from dried Valpolicella grapes: Recioto and Amarone [J].

Celotti, E ;

Ferrarini, R ;

Zironi, R ;

Conte, LS .

JOURNAL OF CHROMATOGRAPHY A, 1996, 730 (1-2) :47-52

[8]

CRAVERO MC, 1995, SEVI, V2557, P2759

[9] PRINCIPAL PHENOLIC PHYTOCHEMICALS IN SELECTED CALIFORNIA WINES AND THEIR ANTIOXIDANT ACTIVITY IN INHIBITING OXIDATION OF HUMAN LOW-DENSITY LIPOPROTEINS [J].

FRANKEL, EN ;

WATERHOUSE, AL ;

TEISSEDRE, PL .

JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 1995, 43 (04) :890-894

[10]

FREGONI M, 1994, VIGNEVINI, V6, P33

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