Pentaamminenitrocobalt(III) dichloride at pressures of 0.24, 0.52, 1.25, 1.91 and 3.38 GPa

被引:15
作者
Boldyreva, EV
Ahsbahs, H
Naumov, DY
Kutoglu, A
机构
[1] SD Russian Acad Sci, Inst Solid State Chem, Novosibirsk 630128, Russia
[2] Univ Marburg, Dept Mineral, D-35032 Marburg, Germany
[3] Univ Marburg, Ctr Mat Sci, D-35032 Marburg, Germany
关键词
D O I
10.1107/S0108270198004879
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The structure of [Co(NO2)(NH3)(5)]Cl-2 has been refined anisotropically from data collected at 0.24, 0.52, 1.25, 1.91 and 3.38 GPa in a diamond anvil cell (DAC). For comparison, the structure of the same crystal in the same DAC was also refined at ambient pressure. The structures at high pressures are anisotropically distorted compared with that at ambient pressure determined in this work and by Bortin [Acta Chem. Scand. (1968), 22, 2890-2898],Kubota & Ohba [Acta Cryst. (1992), B48, 627-632] and Boldyreva et al. [Acta Cryst. (1997c), C53, 523-526], but the space group and the general structural pattern remain the same.
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页码:1378 / 1383
页数:6
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