Rapid synthesis of mesoporous silica with micrometer sized hexagonal prism structure

被引：18

作者：

Wang, LZ ^{[1
]}

Shi, JL ^{[1
]}

Tang, FQ ^{[1
]}

Yu, J ^{[1
]}

Ruan, ML ^{[1
]}

Yan, DS ^{[1
]}

机构：

[1] Chinese Acad Sci, Shanghai Inst Ceram, State Key Lab High Performance Ceram & Superfine, Shanghai 200050, Peoples R China

来源：

JOURNAL OF MATERIALS CHEMISTRY | 1999年 / 9卷 / 03期

关键词：

D O I：

10.1039/a900179d

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

Mesoporous silica MCM-41 material with hexagonal prism structure is rapidly synthesized under strongly acidic condition; accretion of surfactant micellae combined with silica oligomers according to the geometric symmetry of liquid-crystal structure leads to the morphogenesis of the hexagonal structure.

引用

页码：643 / 645

页数：3

共 15 条

[1] A NEW FAMILY OF MESOPOROUS MOLECULAR-SIEVES PREPARED WITH LIQUID-CRYSTAL TEMPLATES [J].

BECK, JS ;

VARTULI, JC ;

ROTH, WJ ;

LEONOWICZ, ME ;

KRESGE, CT ;

SCHMITT, KD ;

CHU, CTW ;

OLSON, DH ;

SHEPPARD, EW ;

MCCULLEN, SB ;

HIGGINS, JB ;

SCHLENKER, JL .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (27) :10834-10843

[2] STUDIES ON MESOPOROUS MATERIALS .1. SYNTHESIS AND CHARACTERIZATION OF MCM-41 [J].

CHEN, CY ;

LI, HX ;

DAVIS, ME .

MICROPOROUS MATERIALS, 1993, 2 (01) :17-26

[3] GENERALIZED SYNTHESIS OF PERIODIC SURFACTANT INORGANIC COMPOSITE-MATERIALS [J].

HUO, QS ;

MARGOLESE, DI ;

CIESLA, U ;

FENG, PY ;

GIER, TE ;

SIEGER, P ;

LEON, R ;

PETROFF, PM ;

SCHUTH, F ;

STUCKY, GD .

NATURE, 1994, 368 (6469) :317-321

[4] ORGANIZATION OF ORGANIC-MOLECULES WITH INORGANIC MOLECULAR-SPECIES INTO NANOCOMPOSITE BIPHASE ARRAYS [J].

HUO, QS ;

MARGOLESE, DI ;

CIESLA, U ;

DEMUTH, DG ;

FENG, PY ;

GIER, TE ;

SIEGER, P ;

FIROUZI, A ;

CHMELKA, BF ;

SCHUTH, F ;

STUCKY, GD .

CHEMISTRY OF MATERIALS, 1994, 6 (08) :1176-1191

[5] ORDERED MESOPOROUS MOLECULAR-SIEVES SYNTHESIZED BY A LIQUID-CRYSTAL TEMPLATE MECHANISM [J].

KRESGE, CT ;

LEONOWICZ, ME ;

ROTH, WJ ;

VARTULI, JC ;

BECK, JS .

NATURE, 1992, 359 (6397) :710-712

[6] Mesoporous molecular sieves MCM-41 with a hollow tubular morphology [J].

Lin, HP ;

Cheng, S ;

Mou, CY .

CHEMISTRY OF MATERIALS, 1998, 10 (02) :581-589

[7] ''Tubules-within-a-tubule'' hierarchical order of mesoporous molecular sieves in MCM-41 [J].

Lin, HP ;

Mou, CY .

SCIENCE, 1996, 273 (5276) :765-768

[8] Sol-gel synthesis of organized matter [J].

Mann, S ;

Burkett, SL ;

Davis, SA ;

Fowler, CE ;

Mendelson, NH ;

Sims, SD ;

Walsh, D ;

Whilton, NT .

CHEMISTRY OF MATERIALS, 1997, 9 (11) :2300-2310

[9] BIOMINERALIZATION AND BIOMIMETIC MATERIALS CHEMISTRY [J].

MANN, S .

JOURNAL OF MATERIALS CHEMISTRY, 1995, 5 (07) :935-946

[10] Synthesis of inorganic materials with complex form [J].

Mann, S ;

Ozin, GA .

NATURE, 1996, 382 (6589) :313-318

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