Transfer of calibration in near-infrared reflectance spectrometry

被引:24
作者
Dreassi, E
Ceramelli, G
Perruccio, PL
Corti, P
机构
[1] Univ Siena, Dept Chem & Pharmaceut Toxicol, I-53100 Siena, Italy
[2] Mil Pharmaceut Estab, I-50144 Florence, Italy
关键词
near-infrared reflectance spectrometry; ranitidine hydrochloride; calibration transfer; chemometrics;
D O I
10.1039/a706694e
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The results of an investigation of the transfer of calibration in near-infrared reflectance spectrometry are reported. Four approaches were tested: direct standardization, direct standardization combined with principal components analysis, ordinary least squares and slope/intercept correction. These approaches were used on two different systems, laboratory samples and industrial samples, for which qualitative and quantitative calibrations had been developed previously, After standardization, the standard error obtained was substantially reduced with respect to the original spectra.
引用
收藏
页码:1259 / 1264
页数:6
相关论文
共 11 条
[1]  
CORTI P, 1992, PHARM ACTA HELV, V67, P57
[2]  
CORTI P, 1992, PROCESS CONTR QUAL, V2, P131
[3]   QUANTITATIVE FOURIER-TRANSFORM NEAR-INFRARED SPECTROSCOPY IN THE QUALITY-CONTROL OF SOLID PHARMACEUTICAL FORMULATIONS [J].
DREASSI, E ;
CERAMELLI, G ;
CORTI, P ;
MASSACESI, M ;
PERRUCCIO, PL .
ANALYST, 1995, 120 (09) :2361-2365
[4]   Application of near-infrared reflectance spectrometry to the analytical control of pharmaceuticals: Ranitidine hydrochloride tablet production [J].
Dreassi, E ;
Ceramelli, G ;
Corti, P ;
Perruccio, PL ;
Lonardi, S .
ANALYST, 1996, 121 (02) :219-222
[5]   NEAR-INFRARED REFLECTANCE SPECTROMETRY IN THE DETERMINATION OF THE PHYSICAL STATE OF PRIMARY MATERIALS IN PHARMACEUTICAL PRODUCTION [J].
DREASSI, E ;
CERAMELLI, G ;
CORTI, P ;
LONARDI, S ;
PERRUCCIO, PL .
ANALYST, 1995, 120 (04) :1005-1008
[6]  
OSBORNE BG, 1983, J FOOD TECHNOL, V18, P453, DOI 10.1177/0047117804048489
[7]  
SCHENK JS, 1985, CROP SCI, V25, P159
[8]  
WANG Y, 1992, ANAL CHEM, V63, P2750
[9]  
WANG Y, 1992, ANAL CHEM, V65, P1301
[10]   CALIBRATION TRANSFER AND MEASUREMENT STABILITY OF NEAR-INFRARED SPECTROMETERS [J].
WANG, YD ;
KOWALSKI, BR .
APPLIED SPECTROSCOPY, 1992, 46 (05) :764-771