The new neutron powder diffractometer with a multi-detector system for high-efficiency and high-resolution measurements

被引:289
作者
Ohoyama, K [1 ]
Kanouchi, T
Nemoto, K
Ohashi, M
Kajitani, T
Yamaguchi, Y
机构
[1] Tohoku Univ, Inst Mat Res, Sendai, Miyagi 98077, Japan
[2] Tohoku Univ, Fac Engn, Sendai, Miyagi 98077, Japan
来源
JAPANESE JOURNAL OF APPLIED PHYSICS PART 1-REGULAR PAPERS SHORT NOTES & REVIEW PAPERS | 1998年 / 37卷 / 6A期
关键词
neutron powder diffraction; crystal structure; magnetic structure; Rietveld profile fitting; diffuse scattering;
D O I
10.1143/JJAP.37.3319
中图分类号
O59 [应用物理学];
学科分类号
摘要
We describe a multipurpose neutron powder diffractometer for high-efficiency and high-resolution measurements, HERMES, which has been installed at the JRR-3M reactor in Japan Atomic Energy Research Institute. To obtain high-quality data for a short counting time, or with a small sample amount, HERMES has a multi-detector system which consists of 150 He-3 neutron detectors and simple window type collimation. The best resolution is Delta 2 theta of 18' and Delta d/d of 3 x 10(-3), where 2 theta and d are scattering-angle and d-spacing, respectively. The duration of an ordinary powder diffraction experiment is 1-5 h under the present conditions in JRR-3M. Some typical results of powder diffraction experiments and performance are given in this paper. We also show a result of 2D intensity mapping of magnetic diffuse scattering from a single crystal of a spin glass material.
引用
收藏
页码:3319 / 3326
页数:8
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