Benzene-1,2,4,5-tetracarboxylic acid dimethyl sulfoxide disolvate: a redetermination at 150 K

被引：4

作者：

Dale, SH ^{[1
]}

Elsegood, MRJ ^{[1
]}

机构：

[1] Loughborough Univ Technol, Dept Chem, Loughborough LE11 3TU, Leics, England

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2003年 / 59卷

关键词：

D O I：

10.1107/S1600536803016295

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

The title compound, C10H6O8.2C(2)H(6)OS, one of the few known examples of the cocrystallization of pyromellitic acid with common organic solvents, has been previously analysed by single-crystal X-ray diffraction at 296 K [Jin, Pan, Shen, Li & Hu (2003). Acta Cryst. C59, o205-o206]. We present here a redetermination at low temperature (150 K). The centrosymmetric compound crystallizes in space group P (1) over bar and exhibits co-operative strong (acid)O - H...O(solvent) and weaker (solvent)C - H...O(acid) hydrogen-bonding interactions, giving rise to a one-dimensional ribbon structure along the bc diagonal of the unit cell.

引用

页码：O1205 / O1207

页数：3

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