Enantioselective syntheses of 13C-labeled (2R)- and (2S)-phytochromobilin dimethyl ester

被引：13

作者：

Jacobi, PA ^{[1
]}

Pippin, D ^{[1
]}

机构：

[1] Dartmouth Coll, Burke Chem Lab, Hanover, NH 03755 USA

来源：

ORGANIC LETTERS | 2001年 / 3卷 / 06期

关键词：

D O I：

10.1021/ol006977q

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

[GRAPHICS] (2R)- and (2S)-phytochromobilin dimethyl ester have been prepared in enantiomerically pure form, specifically C-13-labeled at C-10 or C-15.

引用

页码：827 / 830

页数：4

共 30 条

[1] Probing the photoreaction mechanism of phytochrome through analysis of resonance Raman vibrational spectra of recombinant analogues
Andel, F
Murphy, JT
Haas, JA
McDowell, MT
van der Hoef, I
Lugtenburg, J
Lagarias, JC
Mathies, RA
[J]. BIOCHEMISTRY, 2000, 39 (10) : 2667 - 2676
[2] Excited-state processes in phycocyanobilin studied by femtosecond spectroscopy
Bischoff, M
Hermann, G
Rentsch, S
Strehlow, D
Winter, S
Chosrowjan, H
[J]. JOURNAL OF PHYSICAL CHEMISTRY B, 2000, 104 (08): : 1810 - 1816
[3] THE REACTION OF THIOIMIDES WITH PHOSPHORUS YLIDES
BISHOP, JE
OCONNELL, JF
RAPOPORT, H
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1991, 56 (17) : 5079 - 5091
[4] INVITRO ASSEMBLY OF APOPHYTOCHROME AND APOPHYTOCHROME DELETION MUTANTS EXPRESSED IN YEAST WITH PHYCOCYANOBILIN
DEFORCE, L
TOMIZAWA, KI
ITO, N
FARRENS, D
SONG, PS
FURUYA, M
[J]. PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 1991, 88 (23) : 10392 - 10396
[5] SURFACE-ENHANCED RESONANCE RAMAN-SCATTERING SPECTROSCOPY APPLIED TO PHYTOCHROME AND ITS MODEL COMPOUNDS .2. PHYTOCHROME AND PHYCOCYANIN CHROMOPHORES
FARRENS, DL
HOLT, RE
ROSPENDOWSKI, BN
SONG, PS
COTTON, TM
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1989, 111 (26) : 9162 - 9169
[6] RESONANCE RAMAN ANALYSIS OF THE PR AND PFR FORMS OF PHYTOCHROME
FODOR, SPA
LAGARIAS, JC
MATHIES, RA
[J]. BIOCHEMISTRY, 1990, 29 (50) : 11141 - 11146
[7] FURUYA M, 1987, PHYTOCHROME PHOTOREG
[8] New syntheses of the C,D-ring pyrromethenones of phytochrome and phycocyanin
Jacobi, PA
DeSimone, RW
Ghosh, I
Guo, JS
Leung, SH
Pippin, D
[J]. JOURNAL OF ORGANIC CHEMISTRY, 2000, 65 (25) : 8478 - 8489
[9] Dihydropyrromethenones by Pd(0)-mediated coupling of iodopyrroles and acetylenic amides. Synthesis of the A,B-ring segment of phytochrome
Jacobi, PA
Guo, JS
Rajeswari, S
Zheng, WJ
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1997, 62 (09) : 2907 - 2916
[10] Studies on corrin synthesis. A solution to the introduction of meso substituents
Jacobi, PA
Liu, H
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1999, 64 (06) : 1778 - 1779

← 1 2 3 →