Application of ultrasonic testing to describe the hydration of calcium aluminate cement at the early age

被引:115
作者
Chotard, T [1 ]
Gimet-Breart, N [1 ]
Smith, A [1 ]
Fargeot, D [1 ]
Bonnet, JP [1 ]
Gault, C [1 ]
机构
[1] Ecole Natl Ceram Ind, Grp Etud Mat Heterogenes, F-87065 Limoges, France
关键词
hydration; calcium aluminate cement; ultrasonic measurement; mechanical properties;
D O I
10.1016/S0008-8846(00)00446-4
中图分类号
TU [建筑科学];
学科分类号
0813 ;
摘要
Nondestructive and in situ characterisation techniques, such as ultrasonic measurements, permit to follow cement hydration at the early age from a few minutes to a few hours after mixing. The technique reported in this paper is based on measurements in reflection modes. Results concerning an aluminous cement, Secar71, are presented (water-to-cement weight ratio (WIC): 0.3 and 0.4; temperature of measurement: 20 degreesC; duration: 0-24 h). Information deduced from ultrasonic measurements (longitudinal wave velocity, reflection coefficient) associated with other data obtained from X-ray diffraction (XRD), differential thermal analysis (DTA) and thermogravimetric (TG) measurements enable to propose a qualitative description of hydration's chronology. The sensitivity of these ultrasonic parameters to hydrates formation and structuring is underlined. (C) 2001 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:405 / 412
页数:8
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