Adiabatic single scan two-dimensional NMR spectrocopy

被引：165

作者：

Pelupessy, P ^{[1
]}

机构：

[1] Ecole Normale Super, CNRS, Dept Chim, F-75231 Paris 05, France

来源：

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY | 2003年 / 125卷 / 40期

关键词：

D O I：

10.1021/ja034958g

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

New excitation schemes, based on the use adiabatic pulses, for single scan two-dimensional NMR experiments (Frydman et al., Proc. Nat. Acad. Sci. 2002, 99, 15858-15862) are introduced. The advantages are discussed. Applications in homo- and heteronuclear experiments are presented.

引用

页码：12345 / 12350

页数：6

共 17 条

[1] 2-DIMENSIONAL SPECTROSCOPY - APPLICATION TO NUCLEAR MAGNETIC-RESONANCE [J].

AUE, WP ;

BARTHOLDI, E ;

ERNST, RR .

JOURNAL OF CHEMICAL PHYSICS, 1976, 64 (05) :2229-2246

[2] ABSORPTION-SPECTRA FROM PHASE-MODULATED SPIN ECHOES [J].

BAX, A ;

MEHLKOPF, AF ;

SMIDT, J .

JOURNAL OF MAGNETIC RESONANCE, 1979, 35 (03) :373-377

[3] NATURAL ABUNDANCE N-15 NMR BY ENHANCED HETERONUCLEAR SPECTROSCOPY [J].

BODENHAUSEN, G ;

RUBEN, DJ .

CHEMICAL PHYSICS LETTERS, 1980, 69 (01) :185-189

[4] EXPERIMENTAL ASPECTS OF CHIRP NMR-SPECTROSCOPY [J].

BOHLEN, JM ;

BODENHAUSEN, G .

JOURNAL OF MAGNETIC RESONANCE SERIES A, 1993, 102 (03) :293-301

[5] COHERENCE TRANSFER BY ISOTROPIC MIXING - APPLICATION TO PROTON CORRELATION SPECTROSCOPY [J].

BRAUNSCHWEILER, L ;

ERNST, RR .

JOURNAL OF MAGNETIC RESONANCE, 1983, 53 (03) :521-528

[6] Adjustable, broadband, selective excitation with uniform phase [J].

Cano, KE ;

Smith, MA ;

Shaka, AJ .

JOURNAL OF MAGNETIC RESONANCE, 2002, 155 (01) :131-139

[7] PHASE-SHIFTS INDUCED BY TRANSIENT BLOCH-SIEGERT EFFECTS IN NMR [J].

EMSLEY, L ;

BODENHAUSEN, G .

CHEMICAL PHYSICS LETTERS, 1990, 168 (3-4) :297-303

[8] SELF-REFOCUSING EFFECT OF 270-DEGREES GAUSSIAN PULSES - APPLICATIONS TO SELECTIVE TWO-DIMENSIONAL EXCHANGE SPECTROSCOPY [J].

EMSLEY, L ;

BODENHAUSEN, G .

JOURNAL OF MAGNETIC RESONANCE, 1989, 82 (01) :211-221

[9] The acquisition of multidimensional NMR spectra within a single scan [J].

Frydman, L ;

Scherf, T ;

Lupulescu, A .

PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 2002, 99 (25) :15858-15862

[10] A CONSTANT-TIME C-13-H-1 HSQC WITH UNIFORM EXCITATION OVER THE COMPLETE C-13 CHEMICAL-SHIFT RANGE [J].

HALLENGA, K ;

LIPPENS, GM .

JOURNAL OF BIOMOLECULAR NMR, 1995, 5 (01) :59-66

← 1 2 →