Germanium(II) azides:: synthesis and crystal structure of Tp′GeN3 [Tp′ = hydrotris(3,5-dimethylpyrazol-1-yl)borato]

被引:34
作者
Filippou, AC [1 ]
Portius, P [1 ]
Kociok-Köhn, G [1 ]
机构
[1] Humboldt Univ, Fachinst Anorgan & Allgemeine Chem, D-10115 Berlin, Germany
关键词
D O I
10.1039/a807282e
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The synthesis of the germanium(II) azide Tp'GeN3 (3) from Tp'GeCl (2) [Tp' = HB(3,5-Me(2)pz)(3)] and NaN3 is reported and the crystal structures of 2 and 3 are compared.
引用
收藏
页码:2327 / 2328
页数:2
相关论文
共 23 条
[1]   PHOTOLYTIC REARRANGEMENT OF GERMANIUM AZIDES - EVIDENCE FOR TRANSIENT GERMA-IMINES [J].
BACEIREDO, A ;
BERTRAND, G ;
MAZEROLLES, P .
TETRAHEDRON LETTERS, 1981, 22 (27) :2553-2556
[2]   PHOTOCHEMICAL AND THERMAL REARRANGEMENT OF HEAVIER MAIN-GROUP ELEMENT AZIDES [J].
BERTRAND, G ;
MAJORAL, JP ;
BACEIREDO, A .
ACCOUNTS OF CHEMICAL RESEARCH, 1986, 19 (01) :17-23
[3]   SYNTHESIS AND STRUCTURES OF 2 TRIS(PYRAZOLYL)BORATOTIN(II) COMPOUNDS [J].
COWLEY, AH ;
GEERTS, RL ;
NUNN, CM ;
CARRANO, CJ .
JOURNAL OF ORGANOMETALLIC CHEMISTRY, 1988, 341 (1-3) :C27-C30
[4]   STUDIES IN GERMYL CHEMISTRY .2. EXCHANGE REACTIONS OF SILYL AND GERMYL HALIDES [J].
CRADOCK, S ;
EBSWORTH, EA .
JOURNAL OF THE CHEMICAL SOCIETY A -INORGANIC PHYSICAL THEORETICAL, 1967, (08) :1226-&
[5]   PREPARATION AND CHARACTERIZATION OF PSEUDOHALOGENO(METHYL)GERMANES AND RELATED COMPOUNDS [J].
DRAKE, JE ;
HEMMINGS, RT .
CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1973, 51 (02) :302-311
[6]   APPLICATION OF PHOTOELECTRON-SPECTROSCOPY TO MOLECULAR-PROPERTIES .30. THEORETICAL AND EXPERIMENTAL STUDIES OF THE FLASH PYROLYSIS OF TRIMETHYLSILYL AZIDE AND TRIMETHYLGERMYL AZIDE - GENERATION AND HE-I PHOTOELECTRON-SPECTRA OF IMINOSILYLENE AND IMINOGERMYLENE [J].
GUIMON, C ;
PFISTERGUILLOUZO, G .
ORGANOMETALLICS, 1987, 6 (07) :1387-1392
[7]   Azidotris(trifluoromethyl)germane, (CF3)(3)GeN3: Spectroscopic characterization and density functional computations [J].
Klapotke, TM ;
Schulz, A .
INORGANIC CHEMISTRY, 1996, 35 (17) :4995-4998
[8]   Recent developments in the chemistry of covalent azides [J].
Klapotke, TM .
CHEMISCHE BERICHTE-RECUEIL, 1997, 130 (04) :443-451
[9]  
KOLESNIKOV SP, 1975, CHEM ABSTR 25328U, V82
[10]  
KRICHELDORF HR, 1977, ANGEW CHEM, V89, P570