Fabrication and efficiency evaluation of a hybrid NiCrAl pressure cell up to 4 GPa

被引:60
作者
Fujiwara, Naoki [1 ]
Matsumoto, Takehiko
Koyama-Nakazawa, Kazuko
Hisada, Akihiko
Uwatoko, Yoshiya
机构
[1] Kyoto Univ, Grad Sch Human & Environm Studies, Sakyo Ku, Kyoto 6068501, Japan
[2] Natl Inst Mat Sci, Tsukuba, Ibaraki 3050047, Japan
[3] Univ Tokyo, ISSP, Kashiwa, Chiba 2778581, Japan
关键词
D O I
10.1063/1.2757129
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
A hybrid NiCrAl pressure cell was fabricated to measure magnetic quantities under high pressure above 3 GPa. A pressure of 4.0 GPa was achieved and the pressure cell was found to be reusable even after a pressurizing trial up to 4.0 GPa. Pressure was monitored using Cu-63 nuclear quadrupole resonance of Cu2O and ruby fluorescence. The pressure efficiency of a fresh cell was maintained at 96%, and no appreciable deformation was observed at pressures below 3 GPa; on the other hand, the efficiency after pressurizing trials decreased gradually and reached 75% at 4 GPa accompanied by a maximum expansion inside the cylinder of 2%. (c) 2007 American Institute of Physics.
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页数:5
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