Quantitative analysis of pottery glaze by laser induced breakdown spectroscopy

被引：57

作者：

Yoon, Y

Kim, T

Yang, M

Lee, K

Lee, G

机构：

[1] Korea Inst Geol Mining & Mat, Earth Environ Div, Yusung Ku, Taejon 305350, South Korea

[2] Chungnam Natl Univ, Dept Chem, Yusung Ku, Taejon 305764, South Korea

来源：

MICROCHEMICAL JOURNAL | 2001年 / 68卷 / 2-3期

关键词：

laser induced breakdown spectroscopy; quantitative analysis; pottery glaze;

D O I：

10.1016/S0026-265X(00)00155-7

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

Laser induced breakdown spectroscopy (LIBS) has been applied for the analysis of old pottery glaze. The plasma is generated by focusing a pulsed Nd:YAG laser on the target at air atmospheric pressure. Quantitative analysis was performed on a number of glass bead samples, and a linear calibration curve with a slope of near unity was obtained. The major glaze elements such as Fe, Ca, Mg, Al and Si were analyzed, and the results were compared with X-ray fluorescence method. Elemental analysis showed that the glaze color difference were due to Fe content variation. (C) 2001 Published by Elsevier Science B.V. All rights reserved.

引用

收藏

页码：251 / 256

页数：6

相关论文

共 20 条

[1] DEPTH PROFILE STUDIES USING LASER-INDUCED PLASMA EMISSION-SPECTROMETRY [J].

ANDERSON, DR ;

MCLEOD, CW ;

ENGLISH, T ;

SMITH, AT .

APPLIED SPECTROSCOPY, 1995, 49 (06) :691-701

[2] Laser diagnostics of painted artworks: Laser-induced breakdown spectroscopy in pigment identification [J].

Anglos, D ;

Couris, S ;

Fotakis, C .

APPLIED SPECTROSCOPY, 1997, 51 (07) :1025-1030

[3] Semi-quantitative time resolved LIBS measurements [J].

Barbini, R ;

Colao, F ;

Fantoni, R ;

Palucci, A ;

Ribezzo, S ;

vanderSteen, HJL ;

Angelone, M .

APPLIED PHYSICS B-LASERS AND OPTICS, 1997, 65 (01) :101-107

[4] THE ANALYSIS OF METALS AT A DISTANCE USING LASER-INDUCED BREAKDOWN SPECTROSCOPY [J].

CREMERS, DA .

APPLIED SPECTROSCOPY, 1987, 41 (04) :572-578

[5] Matrix effects in the detection of Pb and Ba in soils using laser-induced breakdown spectroscopy [J].

Eppler, AS ;

Cremers, DA ;

Hickmott, DD ;

Ferris, MJ ;

Koskelo, AC .

APPLIED SPECTROSCOPY, 1996, 50 (09) :1175-1181

[6] On-line monitoring of laser cleaning of limestone by laser-induced breakdown spectroscopy and laser-induced fluorescence [J].

GobernadoMitre, I ;

Prieto, AC ;

Zafiropulos, V ;

Spetsidou, Y ;

Fotakis, C .

APPLIED SPECTROSCOPY, 1997, 51 (08) :1125-1129

[7] QUANTITATIVE ELEMENTAL ANALYSIS OF IRON-ORE BY LASER-INDUCED BREAKDOWN SPECTROSCOPY [J].

GRANT, KJ ;

PAUL, GL ;

ONEILL, JA .

APPLIED SPECTROSCOPY, 1991, 45 (04) :701-705

[8] Laser-induced breakdown spectrometry of titanium dioxide antireflection coatings in photovoltaic cells [J].

Hidalgo, M ;

Martin, F ;

Laserna, JJ .

ANALYTICAL CHEMISTRY, 1996, 68 (07) :1095-1100

[9] Depth profiling of thick layers of graded metal zirconia ceramic coatings using laser ablation inductively coupled plasma atomic emission spectrometry [J].

Kanicky, V ;

Novotny, I ;

Musil, J ;

Mermet, JM .

APPLIED SPECTROSCOPY, 1997, 51 (07) :1042-1046

[10]

Kim T, 1999, J KOREAN PHYS SOC, V35, P198