PIXE elemental mapping on original manuscripts with an external microbeam. Application to manuscripts damaged by iron-gall ink corrosion

被引:37
作者
Remazeilles, C
Quillet, V
Calligaro, T
Dran, JC
Pichon, L
Salomon, J
机构
[1] Univ La Rochelle, Lab Etud Mat Milieux Agressifs, F-17042 La Rochelle 01, France
[2] CNRS, UMR 171, Ctr Rech & Restaurat Musees France, F-75041 Paris 01, France
关键词
iron-gall ink; paper; degradation; PIXE; mapping;
D O I
10.1016/S0168-583X(01)00364-0
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
Proton-induced X-ray emission (PIXE) mapping and PIXE spot analysis have been performed on three original manuscripts. We observed that the precision of the spot measurements for the analysis of the ink composition is limited by the heterogeneity of the writing. PIXE mapping proved to be a complementary technique which is much more sensitive, and which makes it possible to evaluate the migration of some elements, such as sulphur, iron and calcium around inscriptions. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:681 / 687
页数:7
相关论文
共 10 条
[1]   An improved experimental setup for the simultaneous PIXE analysis of heavy and light elements with a 3 MeV proton external beam [J].
Calligaro, T ;
MacArthur, JD ;
Salomon, J .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1996, 109 :125-128
[2]   Development of an external beam nuclear microprobe on the Aglae facility of the Louvre museum [J].
Calligaro, T ;
Dran, JC ;
Ioannidou, E ;
Moignard, B ;
Pichon, L ;
Salomon, J .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 2000, 161 :328-333
[3]   Further results from PIXE analysis of inks in Galileo's notes on motion [J].
DelCarmine, P ;
Giuntini, L ;
Hooper, W ;
Lucarelli, F ;
Mando, PA .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1996, 113 (1-4) :354-358
[4]  
DUVAL A, 1998, 5 INT C NOND TEST MI
[5]   HISTORICAL ANALYSES BY PIXE [J].
KUSKO, BH ;
SCHWAB, RN .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1987, 22 (1-3) :401-406
[6]   Recent applications to the study of ancient inks with the Florence external-PIXE facility [J].
Lucarelli, F ;
Mando, PA .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1996, 109 :644-652
[8]   Ink corrosion aqueous and non-aqueous treatment of paper objects - State of the art [J].
Reissland, B .
RESTAURATOR-INTERNATIONAL JOURNAL FOR THE PRESERVATION OF LIBRARY AND ARCHIVAL MATERIAL, 1999, 20 (3-4) :167-180
[9]   RADIATION-DAMAGE IN PIXE ANALYSIS OF MUSEUM PAPER-LIKE OBJECTS [J].
ZENG, XZ ;
WU, XK ;
SHAO, QY ;
TANG, JY ;
YANG, FJ .
NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS, 1990, 47 (02) :143-147
[10]  
Zerdoun Bat-Yehouda Monique, 1983, ENCRES NOIRES MOYEN