Synchrotron X-ray study of bulk lattice strains in externally loaded Cu-Mo composites

被引:81
作者
Wanner, A [1 ]
Dunand, DC
机构
[1] Univ Stuttgart, Inst Met Kunde, D-70174 Stuttgart, Germany
[2] Northwestern Univ, Dept Mat Sci & Engn, Evanston, IL 60208 USA
来源
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE | 2000年 / 31卷 / 11期
基金
美国能源部; 美国国家科学基金会;
关键词
D O I
10.1007/BF02830344
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A synchrotron X-ray transmission technique was applied to study the internal load transfer and micromechanical damage in molybdenum particle-reinforced copper matrix composites during plastic deformation. Mechanically loaded, 1.5-mm-thick specimens were irradiated with a monochromatic beam of 65 keV X-rays. Low-index diffraction rings of both phases were recorded with a high-resolution two-dimensional detector. By means of newly developed data processing routines, we could quantify as a function of applied stress both the ring distortion (from which the volume-averaged elastic strains in the two phases were calculated), and the ring graininess (which is related to the Bragg peak broadening). Based on this information, the deformation and damage processes in these alloys were studied in detail. As compared to conventional neutron diffraction methods, the photon transmission technique yielded similar precision but at much reduced measurement times. The main sources of experimental errors were identified and strategies to minimize these errors were developed.
引用
收藏
页码:2949 / 2962
页数:14
相关论文
共 26 条
[1]   THE ANALYSIS OF INTERNAL STRAINS MEASURED BY NEUTRON-DIFFRACTION IN AL-SIC METAL MATRIX COMPOSITES [J].
ALLEN, AJ ;
BOURKE, MAM ;
DAWES, S ;
HUTCHINGS, MT ;
WITHERS, PJ .
ACTA METALLURGICA ET MATERIALIA, 1992, 40 (09) :2361-2373
[2]  
[Anonymous], 1977, DIFFRACTION MAT
[3]   MEASUREMENT AND PREDICTION OF STRAIN IN INDIVIDUAL PHASES OF A 2219AL/TIC/15P-T6 COMPOSITE DURING LOADING [J].
BOURKE, MAM ;
GOLDSTONE, JA ;
SHI, N ;
ALLISON, JE ;
STOUT, MG ;
LAWSON, AC .
SCRIPTA METALLURGICA ET MATERIALIA, 1993, 29 (06) :771-776
[4]  
Boyer H, 1987, ATLAS STRESS STRAIN
[5]  
Clyne T.W., 1993, INTRO METAL MATRIX C
[6]  
COURTHEY TH, 1990, MECH BEHAV MAT, P59
[7]   Elastic phase-strain distribution in a particulate-reinforced metal-matrix composite deforming by slip or creep [J].
Daymond, MR ;
Lund, C ;
Bourke, MAM ;
Dunand, DC .
METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1999, 30 (11) :2989-2997
[8]   A synchrotron radiation study of transient internal strain changes during the early stages of thermal cycling in an Al/SiCW MMC [J].
Daymond, MR ;
Withers, PJ .
SCRIPTA MATERIALIA, 1996, 35 (10) :1229-1234
[9]   Use of Rietveld refinement for elastic macrostrain determination and for evaluation of plastic strain history from diffraction spectra [J].
Daymond, MR ;
Bourke, MAM ;
VonDreele, RB ;
Clausen, B ;
Lorentzen, T .
JOURNAL OF APPLIED PHYSICS, 1997, 82 (04) :1554-1562
[10]   Use of Rietveld refinement to fit a hexagonal crystal structure in the presence of elastic and plastic anisotropy [J].
Daymond, MR ;
Bourke, MAM ;
Von Dreele, RB .
JOURNAL OF APPLIED PHYSICS, 1999, 85 (02) :739-747