NMR spectroscopy and atomic force microscopy characterization of hybrid organic-inorganic coatings

被引：2

作者：

Brus, J ^{[1
]}

Spírková, M ^{[1
]}

机构：

[1] Acad Sci Czech Republ, Inst Macromol Chem, CR-16206 Prague, Czech Republic

来源：

MACROMOLECULAR SYMPOSIA | 2005年 / 220卷

关键词：

atomic force microscopy; coatings and films; solid-state NMR;

D O I：

10.1002/masy.200550212

中图分类号：

O63 [高分子化学（高聚物）];

学科分类号：

070305 ; 080501 ; 081704 ;

摘要：

Hybrid organic-inorganic (O-I) epoxide-based products made from functionalized organosilicon precursors, oligomeric di- and triamines and in some cases colloidal silica particles were characterized by NMR spectroscopy and atomic force microscopy (AFM). The kinetics and reaction mechanism of condensation reactions, structure and segmental dynamics of final films, as well as homogeneity and partial ordering were studied by solid-state NMR spectroscopy (2D CRAMPS, 2D H-1-C-13 WISE, relaxation experiments); the surface morphology and other surface characteristics were determined by AFM.

引用

页码：155 / 164

页数：10

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