The behaviour of polydentate hydrazonic ligands derived from 2-acetylpyridine towards organotin compounds Part II. The monoorganotin(IV) complexes

被引：29

作者：

Carcelli, M

Fochi, A

Pelagatti, P

Pelizzi, G

Russo, U

机构：

[1] Univ Parma, Dipartimento Chim Gen & Inorgan, I-43100 Parma, Italy

[2] Univ Padua, Dipartimento Chim Inorgan Metallorgan & Anali, I-35131 Padua, Italy

来源：

JOURNAL OF ORGANOMETALLIC CHEMISTRY | 2001年 / 626卷 / 1-2期

关键词：

organotin compounds; polydentate ligands; sulphur ligands; pyridyl ligands;

D O I：

10.1016/S0022-328X(01)00677-5

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

The study of the reactivity of the ligands bis(2-acetylpyridine)thiocarbonohydrazone (H(2)apt), 2-acetylpyridine thiosemicarbazone (Hapts) and 2-acetylpyridine semicarbazone (Haps) towards monoorganotin(IV) compounds was carried out; all the new derivatives were spectroscopically (IR, H-1-NMR and Mossbauer) characterised. The X-ray crystal structures of [(n-Bu)Sn(Hapt)Cl-2]. 5H(2)o, [PhSn(Hapt)Cl-2].C2H5OH .H2O and [PhSn(aps)Cl-2] were reported and a comparison was made with the already characterised diorganotin complexes of the same ligands. (C) 2001 Elsevier Science B.V. All rights reserved.

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页码：161 / 167

页数：7

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