Levels of PCDDs, PCDFs and non-ortho PCBs in dietary supplement fish oil obtained in Spain.

被引:28
作者
Jimenez, B [1 ]
Wright, C [1 ]
Kelly, M [1 ]
Startin, JR [1 ]
机构
[1] MAFF,FOOD SAFETY DIRECTORATE,CENT SCI LAB,NORWICH NR4 7UQ,NORFOLK,ENGLAND
关键词
D O I
10.1016/0045-6535(95)00233-2
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Levels of PCDDs, PCDFs and non-ortho PCBs are reported for fish oils available in Spain which are consumed by the population as a dietary supplement. Trace enrichment methodology based on the use of modified silica and activated carbon chromatography was combined wiht on-column extraction (FMS 100) to separate PCDDs, PCDFs and PCBs from lipid material. The extracts were further cleaned up on disposable Florisil columns and analysed by HRGC/HRMS (PCDD/F and non-ortho PCB fractions). Mean levels found in the samples were 10.50 ppt for total PCDDs and 9.95 ppt for total PCDFs. Calculated PCDD/F I-TEQ values were found to be 2.11 ppt on a lipid weight basis. Total mean levels found for co-planar PCBs (# 77, 126 and 169) were 18.26 ppt and the calculated I-TEQ value was 0.31 ppt on a lipid weight basis.
引用
收藏
页码:461 / 467
页数:7
相关论文
共 17 条
[1]   PCDD AND PCDF BODY BURDEN FROM FOOD-INTAKE IN THE FEDERAL-REPUBLIC OF GERMANY [J].
BECK, H ;
ECKART, K ;
MATHAR, W ;
WITTKOWSKI, R .
CHEMOSPHERE, 1989, 18 (1-6) :417-424
[2]   AIRBORNE DIOXINS AND DIBENZOFURANS - SOURCES AND FATES [J].
CZUCZWA, JM ;
HITES, RA .
ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1986, 20 (02) :195-200
[3]   LEVELS OF PCDDS AND PCDFS IN FOODSTUFFS FROM THE FEDERAL-REPUBLIC-OF-GERMANY [J].
FURST, P ;
FURST, C ;
GROEBEL, W .
CHEMOSPHERE, 1990, 20 (7-9) :787-792
[4]  
GONZALEZ MJ, 1993, CHEMOSPHERE, V27, P97, DOI 10.1016/0045-6535(93)90281-9
[5]  
GONZALEZ MJ, 1993, ORGANOHALOGEN COMPOU, V13
[6]   PRESENCE OF PCDDS AND PCDFS IN FOOD FOR HUMAN CONSUMPTION - A REVIEW [J].
JIMENEZ, B ;
GONZALEZ, MJ ;
HERNANDEZ, LM .
FOOD CHEMISTRY, 1991, 39 (03) :257-271
[7]  
JIMENEZ B, 1993, ORGANOHALOGEN COMPOU, V13
[8]  
KROKOS F, 1995, UNPUB CONGENER SPECI
[9]  
KROKOS F, 1993, ORGANOHALOGEN COMPOU, V11
[10]  
*NATO, 1988, 176 N ATL TREAT ORG