Anodic electrochemistry and the use of a 6-volt lantern battery: A simple method for attempting electrochemically based synthetic transformations

被引:49
作者
Frey, DA [1 ]
Wu, N [1 ]
Moeller, KD [1 ]
机构
[1] WASHINGTON UNIV,DEPT CHEM,ST LOUIS,MO 63130
关键词
D O I
10.1016/0040-4039(96)01946-6
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A series of electrochemical transformations have been accomplished using a 6-volt lantern battery as a power supply. The reactions included both intramolecular anodic olefin coupling reactions and an anodic amide oxidation. In all cases, the reactions afforded preparatively useful amounts of product and demonstrated that electrochemical synthetic methods can be readily attempted without the need for specialized equipment. Copyright (C) 1996 Elsevier Science Ltd
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页码:8317 / 8320
页数:4
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