STRUCTURAL INVESTIGATION OF BACTERIAL LIPOPOLYSACCHARIDES BY MASS SPECTROMETRY AND TANDEM MASS SPECTROMETRY

被引：55

作者：

Banoub, Joseph H. ^{[1
,2
]}

El Aneed, Anas ^{[3
]}

Cohen, Alejandro M. ^{[1
,2
]}

Joly, Nicolas ^{[4
]}

机构：

[1] Fisheries & Oceans Canada, Sci Branch, Special Projects, St John, NF A1C 5X1, Canada

[2] Mem Univ Newfoundland, Dept Chem, St John, NF A1B 3V6, Canada

[3] Univ Saskatchewan, Coll Pharm & Nutr, Saskatoon, SK S7N 5C9, Canada

[4] IUT Bethune, Unite Catalyse & Chim Solide, CNRS, Dept Chim,UMR 8181, F-62408 Bethune, France

来源：

MASS SPECTROMETRY REVIEWS | 2010年 / 29卷 / 04期

基金：

加拿大自然科学与工程研究理事会;

关键词：

MS and MS/MS analyses; O-antigen; LPS; core oligosaccharide; lipid A; O-SPECIFIC POLYSACCHARIDE; INNER-CORE REGION; PSEUDOALTEROMONAS-HALOPLANKTIS TAC-125; SUBSP SALMONICIDA LIPOPOLYSACCHARIDE; ESCHERICHIA-COLI LIPOPOLYSACCHARIDE; POLYACRYLAMIDE GEL-ELECTROPHORESIS; O1K2; NCTC-5055; LIPOPOLYSACCHARIDE; KLEBSIELLA-PNEUMONIAE SEROTYPE-O1; REDUCING END GROUP; LIPID-A;

D O I：

10.1002/mas.20258

中图分类号：

O433 [光谱学];

学科分类号：

070207 [光学];

摘要：

Mass spectrometric studies are now playing a leading role in the elucidation of lipopolysaccharide (LPS) structures through the characterization of antigenic polysaccharides, core oligosaccharides and lipid A components including LPS genetic modifications. The conventional MS and MS/MS analyses together with CID fragmentation provide additional structural information complementary to the previous analytical experiments, and thus contribute to an integrated strategy for the simultaneous characterization and correct sequencing of the carbohydrate moiety. (C) 2010 Wiley Periodicals, Inc., Mass Spec Rev 29:606-650, 2010

引用

页码：606 / 650

页数：45

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