Spherical MCM-41 as support material in enantioselective HPLC

被引:41
作者
Thoelen, C [1 ]
Paul, J [1 ]
Vankelecom, IFJ [1 ]
Jacobs, PA [1 ]
机构
[1] Katholieke Univ Leuven, Fac Agr & Appl Biol Sci, Ctr Surface Chem & Catalysis, B-3001 Louvain, Belgium
关键词
D O I
10.1016/S0957-4166(00)00439-0
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
Spherical MCM-41 particles covalently linked with (R)-naphthylethylamine as selector are reported as a new chiral stationary phase for HPLC and show excellent resolution and efficiency in combination with low inlet pressures. (C) 2001 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码:4819 / 4823
页数:5
相关论文
共 10 条
[1]   STRUCTURAL CHARACTERIZATION OF (3-AMINOPROPYL)TRIETHOXYSILANE-MODIFIED SILICAS BY SI-29 AND C-13 NUCLEAR MAGNETIC-RESONANCE [J].
CARAVAJAL, GS ;
LEYDEN, DE ;
QUINTING, GR ;
MACIEL, GE .
ANALYTICAL CHEMISTRY, 1988, 60 (17) :1776-1786
[2]   Optimal parameters for the synthesis of the mesoporous molecular sieve [Si]-MCM-41 [J].
Cheng, CF ;
Park, DH ;
Klinowski, J .
JOURNAL OF THE CHEMICAL SOCIETY-FARADAY TRANSACTIONS, 1997, 93 (01) :193-197
[3]  
FRANKE O, 1994, STUD SURF SCI CATAL, V84, P77
[4]   The synthesis of micrometer- and submicrometer-size spheres of ordered mesoporous oxide MCM-41 [J].
Grun, M ;
Lauer, I ;
Unger, KK .
ADVANCED MATERIALS, 1997, 9 (03) :254-&
[5]   Comparison of an ordered mesoporous aluminosilicate, silica, alumina, titania and zirconia in normal-phase high-performance liquid chromatography [J].
Grun, M ;
Kurganov, AA ;
Schacht, S ;
Schuth, F ;
Unger, KK .
JOURNAL OF CHROMATOGRAPHY A, 1996, 740 (01) :1-9
[6]   Packings of an unidimensional regular pore structure as model packings in size-exclusion and inverse size-exclusion chromatography [J].
Kurganov, A ;
Unger, K ;
Issaeva, T .
JOURNAL OF CHROMATOGRAPHY A, 1996, 753 (02) :177-190
[7]   HIGH-PERFORMANCE LIQUID-CHROMATOGRAPHIC SEPARATION OF ENANTIOMERS ON (S)-1-(ALPHA-NAPHTHYL)ETHYLAMINE BONDED TO SILICA-GEL [J].
OI, N ;
NAGASE, M ;
DOI, T .
JOURNAL OF CHROMATOGRAPHY, 1983, 257 (01) :111-117
[8]   Mesoporous M41S materials in capillary gas chromatography [J].
Raimondo, M ;
Perez, G ;
Sinibaldi, N ;
DeStefanis, A ;
Tomlinson, AAG .
CHEMICAL COMMUNICATIONS, 1997, (15) :1343-1344
[9]   CONTROLLED GROWTH OF MONODISPERSE SILICA SPHERES IN MICRON SIZE RANGE [J].
STOBER, W ;
FINK, A ;
BOHN, E .
JOURNAL OF COLLOID AND INTERFACE SCIENCE, 1968, 26 (01) :62-&
[10]   The use of M41S materials in chiral HPLC [J].
Thoelen, C ;
Van de Walle, K ;
Vankelecom, IFJ ;
Jacobs, PA .
CHEMICAL COMMUNICATIONS, 1999, (18) :1841-1842