Recent developments in solid-state nuclear magnetic resonance of quadrupolar nuclei and applications to biological systems

被引:53
作者
Wu, G [1 ]
机构
[1] Queens Univ, Dept Chem, Kingston, ON K7L 3N6, Canada
关键词
nuclear magnetic resonance; quadrupole; solid state; biological system;
D O I
10.1139/bcb-76-2-3-429
中图分类号
Q5 [生物化学]; Q7 [分子生物学];
学科分类号
071010 ; 081704 ;
摘要
Recent advances in nuclear magnetic resonance (NMR) methodology and improvements in high-field NMR instrumentation have generated a new wave of research interests in the application of solid-state NMR to the study of quadrupolar nuclei. These developments now permit increasingly complex biological systems to be probed by quadrupolar NMR. In this review I describe a few recent developments in NMR studies of quadrupolar nuclei and demonstrate the potential of solid-state quadrupolar NMR in the study of biological systems. In particular, I discuss the application of solid-state NMR of O-17, Zn-67, Co-59, Na-23, and K-39 nuclei with a prognosis for future work.
引用
收藏
页码:429 / 442
页数:14
相关论文
共 119 条
[1]   STRUCTURE OF RHOMBOHEDRAL 2 ZINC INSULIN CRYSTALS [J].
ADAMS, MJ ;
BLUNDELL, TL ;
DODSON, EJ ;
DODSON, GG ;
VIJAYAN, M ;
BAKER, EN ;
HARDING, MM ;
HODGKIN, DC ;
RIMMER, B ;
SHEAT, S .
NATURE, 1969, 224 (5218) :491-&
[2]   Synthesis of (N-15(2))[O-17]urea, (N-15(2))[O-2,O-4-O-17(2)]uridine, and (N-15(3))[O-2-O-17]cytidine [J].
Amantea, A ;
Henz, M ;
Strazewski, P .
HELVETICA CHIMICA ACTA, 1996, 79 (01) :244-254
[3]   Z filtering in MQMAS NMR [J].
Amoureux, JP ;
Fernandez, C ;
Steuernagel, S .
JOURNAL OF MAGNETIC RESONANCE SERIES A, 1996, 123 (01) :116-118
[4]   Optimized multiple-quantum magic-angle spinning NMR experiments on half-integer quadrupoles [J].
Amoureux, JP ;
Fernandez, C ;
Frydman, L .
CHEMICAL PHYSICS LETTERS, 1996, 259 (3-4) :347-355
[5]   GALLIUM(3+) BINDING TO OVOTRANSFERRIN AND ITS HALF-MOLECULES - A MULTINUCLEAR NMR-STUDY [J].
ARAMINI, JM ;
MCINTYRE, DD ;
VOGEL, HJ .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1994, 116 (25) :11506-11511
[6]   FIELD-DEPENDENT AL-27 NMR-STUDIES OF THE TRANSFERRINS - AN APPROACH FOR THE STUDY OF METAL-ION BINDING-SITES IN LARGER PROTEINS [J].
ARAMINI, JM ;
GERMANN, MW ;
VOGEL, HJ .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1993, 115 (21) :9750-9753
[7]   AL-27 AND C-13 NMR-STUDIES OF ALUMINUM(3+) BINDING TO OVOTRANSFERRIN AND ITS HALF-MOLECULES [J].
ARAMINI, JM ;
VOGEL, HJ .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1993, 115 (01) :245-252
[8]   A SC-45 NMR-STUDY OF OVOTRANSFERRIN AND ITS HALF-MOLECULES [J].
ARAMINI, JM ;
VOGEL, HJ .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1994, 116 (05) :1988-1993
[9]   Factors controlling the O-17 NMR chemical shift in ionic mixed metal oxides [J].
Bastow, TJ ;
Dirken, PJ ;
Smith, ME ;
Whitfield, HJ .
JOURNAL OF PHYSICAL CHEMISTRY, 1996, 100 (47) :18539-18545
[10]   NUCLEAR MAGNETIC RESONANCE POWDER PATTERNS IN PRESENCE OF COMPLETELY ASYMMETRIC QUADRUPOLE AND CHEMICAL SHIFT EFFECTS - APPLICATION TO METAVANADATES [J].
BAUGHER, JF ;
TAYLOR, PC ;
OJA, T ;
BRAY, PJ .
JOURNAL OF CHEMICAL PHYSICS, 1969, 50 (11) :4914-&