Harmonisation and quality assurance in pre-analytical steps of soil contamination studies - conclusions and recommendations of the CEEM Soil project

被引:17
作者
Wagner, G [1 ]
Desaules, A
Muntau, H
Theocharopoulos, S
Quevauviller, P
机构
[1] Univ Saarland, Inst Biogeog, D-66041 Saarbrucken, Germany
[2] Inst Environm Protect & Agr, Swiss Fed Res Stn Agroecol & Agr, CH-3003 Bern, Switzerland
[3] Commiss European Communities, Joint Res Ctr, Inst Environm, I-21020 Ispra, Italy
[4] Natl Agr Res Fdn, Soil Sci Inst Athens, Athens 14123, Greece
[5] Commiss European Communities, SM&T, DG 12, B-1049 Brussels, Belgium
关键词
soil sampling; sample pre-treatment; comparability; standardisation; harmonisation; soil contamination studies; monitoring; quality assurance; quality control; accreditation;
D O I
10.1016/S0048-9697(00)00614-8
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
The paper summarises the project's results and consequences including expert's statements. Based on sampling strategies and methodological details which have been recognised to be critical for the comparability of the results of soil contamination studies, recommendations are given towards harmonisation of soil sampling guidelines, improvement of quality assurance of pre-analytical steps and inclusion of soil sampling into accreditation systems. Recommended approaches to improve QA and QC in soil sampling are: harmonised guidelines; specified SOPs; written sampling (strategy) plans; defined qualification and experience of sampling personnel; sampling records; regular interlaboratory comparisons (proficency tests) for sampling; and inclusion of sampling and sample preparation into accreditation procedures. Needs for further research in the field of pre-analytical phases of soil contamination studies are outlined and further R&D projects are encouraged. (C) 2001 Elsevier Science B.V. All rights reserved.
引用
收藏
页码:103 / 117
页数:15
相关论文
共 25 条
[1]   The evaluation of measurement uncertainty from method validation studies - Part 1: Description of a laboratory protocol [J].
Barwick, VJ ;
Ellison, SLR .
ACCREDITATION AND QUALITY ASSURANCE, 2000, 5 (02) :47-53
[2]   Geostatistical analysis of sampling uncertainty at the Tollesbury Managed Retreat site in Blackwater Estuary, Essex, UK: Kriging and cokriging approach to minimise sampling density [J].
Chang, YH ;
Scrimshaw, MD ;
Emmerson, RHC ;
Lester, JN .
SCIENCE OF THE TOTAL ENVIRONMENT, 1998, 221 (01) :43-57
[3]  
CLINE MG, 1944, UNIT SOIL SCI SOC AM, V8, P275
[4]  
COFINO WP, 1994, AKKREDITIERUNG QUALI, P173
[5]   Description of the test area and reference sampling at Dornach [J].
Desaules, A ;
Sprengart, J ;
Wagner, G ;
Muntau, H ;
Theocharopoulos, S .
SCIENCE OF THE TOTAL ENVIRONMENT, 2001, 264 (1-2) :17-26
[6]  
GORLITZ G, 1994, QUALITAT ANAL LABOR, P159
[7]  
*ISO, 1995, 5725 ISO
[8]  
*ISO DIS, 1995, 103812 ISODIS
[9]  
*ISO DIS, 1997, 110742 ISODIS
[10]  
*ISO DIS, 2000, 103815 ISODIS