Proton-proton constraints in powdered solids from 1H-1H-1H and 1H-1H-13C three-dimensional NMR chemical shift correlation spectroscopy

被引:29
作者
Sakellariou, D [1 ]
Lesage, A [1 ]
Emsley, L [1 ]
机构
[1] Ecole Normale Super Lyon, Lab Stereochim & Interact Mol, UMR 5532 CNRS, F-69364 Lyon, France
关键词
D O I
10.1021/ja005846h
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
引用
收藏
页码:5604 / 5605
页数:2
相关论文
共 19 条
[1]   HETERONUCLEAR DECOUPLING IN ROTATING SOLIDS [J].
BENNETT, AE ;
RIENSTRA, CM ;
AUGER, M ;
LAKSHMI, KV ;
GRIFFIN, RG .
JOURNAL OF CHEMICAL PHYSICS, 1995, 103 (16) :6951-6958
[2]   FREQUENCY-SWITCHED PULSE SEQUENCES - HOMONUCLEAR DECOUPLING AND DILUTE SPIN NMR IN SOLIDS [J].
BIELECKI, A ;
KOLBERT, AC ;
LEVITT, MH .
CHEMICAL PHYSICS LETTERS, 1989, 155 (4-5) :341-346
[3]  
Bielecki A., 1990, ADV MAGN RESON, V14, P111, DOI [10.1016/b978-0-12-025514-6.50011-3, DOI 10.1016/B978-0-12-025514-6.50011-3]
[4]   CHARACTERIZATION OF HETEROGENEOUS POLYMER BLENDS BY 2-DIMENSIONAL PROTON SPIN DIFFUSION SPECTROSCOPY [J].
CARAVATTI, P ;
NEUENSCHWANDER, P ;
ERNST, RR .
MACROMOLECULES, 1985, 18 (01) :119-122
[5]   Multi-dimensional 1H NMR nuclear Overhauser spectroscopy under magic angle spinning:: theory and application to elastomers [J].
Fritzhanns, T ;
Demco, DE ;
Hafner, S ;
Spiess, HW .
MOLECULAR PHYSICS, 1999, 97 (08) :931-943
[6]   Dipolar couplings and internuclear distances by double-quantum nuclear magnetic resonance spectroscopy of solids [J].
Graf, R ;
Demco, DE ;
Gottwald, J ;
Hafner, S ;
Spiess, HW .
JOURNAL OF CHEMICAL PHYSICS, 1997, 106 (03) :885-895
[7]   Hydrogen bonding and distance studies of amino acids and peptides using solid state 2D H-1-C-13 heteronuclear correlation spectra [J].
Gu, ZT ;
Ridenour, CF ;
Bronnimann, CE ;
Iwashita, T ;
McDermott, A .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1996, 118 (04) :822-829
[8]  
Haeberlen U., 1976, HIGH RESOLUTION N S1
[9]   Carbon-proton chemical shift correlation in solid-state NMR by through-bond multiple-quantum spectroscopy [J].
Lesage, A ;
Sakellariou, D ;
Steuernagel, S ;
Emsley, L .
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1998, 120 (50) :13194-13201
[10]   Through-bond heteronuclear single-quantum correlation spectroscopy in solid-state NMR, and comparison to other through-bond and through-space experiments [J].
Lesage, A ;
Emsley, L .
JOURNAL OF MAGNETIC RESONANCE, 2001, 148 (02) :449-454