End-shaped copper fibers in an epoxy matrix - predicted versus actual fracture toughening

End-shaped copper fibers are placed in a brittle thermoset epoxy matrix at 10 vol% and tested in four-point bending to determine the fracture toughness of the composite. Results from four-point bend tests agree well with the theoretical predictions of the fracture toughness increment 'Delta G' of a metal fiber/brittle thermoset matrix composite based on single fiber pullout (SFP) tests. This close agreement demonstrates that SFP testing, along with the theoretical model, can be used as an effective end-shape screening tool for ductile fibers before full scale composite testing. The model predicts that the composite's fracture toughness will be 46% higher with flat end-impacted fibers and 4% lower with rippled fibers compared to straight fibers at a 0 degrees orientation. Four-point bend results show the actual composite's fracture toughness is 49% higher with flat end-impacted fibers and 5% lower with rippled fibers compared to straight fibers. Further, four-point bend results show that end-shaped copper fibers improve both the flexural strength and modulus of the composite, demonstrating that end-shaped ductile fibers provide a good stress transfer to the fibers by anchoring the fibers into the matrix. Lastly, experimental validation of the model also indicates that at low fiber volume fractions, fiber-fiber interaction has only a minor influence on the fracture toughness for the tested ductile fiber/brittle matrix composite. (c) 2005 Elsevier Ltd. All rights reserved.