Implementation of a temperature-gradient reactor system for high-throughput investigation of phosphonate-based inorganic-organic hybrid compounds

被引：72

作者：

Bauer, Sebastian ^{[1
]}

Stock, Norbert ^{[1
]}

机构：

[1] Univ Kiel, Inst Anorgan Chem, D-24098 Kiel, Germany

来源：

ANGEWANDTE CHEMIE-INTERNATIONAL EDITION | 2007年 / 46卷 / 36期

关键词：

combinatorial chemistry; high-throughput screening; hydrothermal synthesis; inorganic-organic compounds; phosphonates;

D O I：

10.1002/anie.200701575

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

(Graph Presented) Five new Cd phosphonates were discovered in a systematic investigation of the influence of the reaction temperature besides composition and pH value on the synthesis of inorganic-organic hybrid compounds in the CdCl2/H5L/NaOH system, which was achieved by the title procedure. In the resulting crystallization diagram (see picture), each color corresponds to a different phase. © 2007 Wiley-VCH Verlag GmbH & Co. KGaA.

引用

页码：6857 / 6860

页数：4

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