Determination of trace amounts of Galaxolide® (HHCB) by HPLC

被引:6
作者
Schussler, W [1 ]
Nitschke, L [1 ]
机构
[1] Bayer Landesamt Wasserwirtschaft, Inst Wasserforsch, D-80539 Munich, Germany
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 1998年 / 361卷 / 02期
关键词
Acetic; HPLC; Acetic Acid; Acetonitrile; Detection Limit;
D O I
10.1007/s002160050867
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
An analytical method for the determination of trace amounts of Galaxolide(R) (HHCB) by HPLC is presented. It is based on the separation of HHCB in different samples by a C18-column and a gradient elution by water and acetonitrile, both containing some acetic acid. The detection is carried out with a combination of a fast scanning UV detector and a fast scanning fluorescence detector. The fluorescence detection limit is 5 mu g/L HHCB without sample pretreatment. HHCB adsorbed on solids or suspended solids can be extracted by ethanol.
引用
收藏
页码:220 / 221
页数:2
相关论文
共 2 条
[1]  
ESCHKE HD, 1994, Z UMWELTCHEM OKOTOX, V6, P183
[2]  
Ohloff G., 1990, RIECHSTOFFE GERUCHSS