Extraction, preparation and characterization of cellulose fibres and nanocrystals from rice husk

被引：1147

作者：

Johar, Nurain ^{[1
,2
]}

Ahmad, Ishak ^{[1
,2
]}

Dufresne, Alain ^{[3
]}

机构：

[1] Univ Kebangsaan Malaysia, Fac Sci & Technol, Polymer Res Ctr PORCE, Bangi 43600, Selangor, Malaysia

[2] Univ Kebangsaan Malaysia, Fac Sci & Technol, Sch Chem Sci & Food Technol, Bangi 43600, Selangor, Malaysia

[3] Grenoble Inst Technol, Int Sch Paper Print Media & Biomat Pagora, F-38402 St Martin Dheres, France

来源：

INDUSTRIAL CROPS AND PRODUCTS | 2012年 / 37卷 / 01期

关键词：

Rice husk; Natural fibres; Purification; Cellulose nanocrystals; FLAX STRAW FIBERS; MECHANICAL-PROPERTIES; WHEAT-STRAW; SILICA; NANOFIBERS; HYDROLYSIS; WHISKERS;

D O I：

10.1016/j.indcrop.2011.12.016

中图分类号：

S2 [农业工程];

学科分类号：

082806 [农业信息与电气工程];

摘要：

Cellulose fibres and cellulose nanocrystals were extracted from rice husk. Fibres were obtained by submitting the industrial rice crop to alkali (NaOH) and bleaching treatments. Nanocrystals were extracted from these fibres using sulphuric acid (H2SO4) hydrolysis treatment. The material obtained after each stage of the treatments was carefully characterized and its chemical composition was determined. Morphological investigation was performed using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). Fourier transform infrared (FTIR) spectroscopy showed the progressive removal of non-cellulosic constituents. X-ray diffraction (XRD) analysis revealed that the crystallinity increased with successive treatments. The thermal stability of the rice husk fibres and cellulose nanocrystals was also investigated using thermogravimetric analysis (TGA). (c) 2011 Elsevier B.V. All rights reserved.

引用

页码：93 / 99

页数：7

共 39 条

[1]

Ahmad I, 2007, IRAN POLYM J, V16, P233

[2]

Biocomposites from wheat straw nanofibers: Morphology, thermal and mechanical properties [J].

Alemdar, Ayse ;

Sain, Mohini .

COMPOSITES SCIENCE AND TECHNOLOGY, 2008, 68 (02) :557-565

[3]

Isolation and characterization of nanofibers from agricultural residues - Wheat straw and soy hulls [J].

Alemdar, Ayse ;

Sain, Mohini .

BIORESOURCE TECHNOLOGY, 2008, 99 (06) :1664-1671

[4]

[Anonymous], 1984, WOOD CHEM ULTRASTRUC, DOI DOI 10.1515/9783110839654

[5]

Chemical and morphological characteristics of Malaysian cultivated kenaf (Hibiscus cannabinus) fiber [J].

Ashori, A ;

Harun, J ;

Raverty, WD ;

Yusoff, MNM .

POLYMER-PLASTICS TECHNOLOGY AND ENGINEERING, 2006, 45 (01) :131-134

[6]

Batra S.K., 1981, HDB FIBER SCI TECHNO, V4

[7]

Bhanumathidas N., 2004, INT C PROCEEDING 7 C, V1, P379, DOI [10.14359/10505, DOI 10.14359/10505]

[8]

Processing of cellulose nanofiber-reinforced composites [J].

Bhatnagar, A ;

Sain, M .

JOURNAL OF REINFORCED PLASTICS AND COMPOSITES, 2005, 24 (12) :1259-1268

[9]

Processing, properties and applications of reactive silica from rice husk - an overview [J].

Chandrasekhar, S ;

Satyanarayana, KG ;

Pramada, PN ;

Raghavan, P ;

Gupta, TN .

JOURNAL OF MATERIALS SCIENCE, 2003, 38 (15) :3159-3168

[10]

Rice husk ash as an alternate source for active silica production [J].

Della, VP ;

Kühn, I ;

Hotza, D .

MATERIALS LETTERS, 2002, 57 (04) :818-821

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