An efficient procedure for the esterification of nitroacetic acid: Application to the preparation of Merrifield resin-bound nitroacetate

被引：16

作者：

Sylvain, C ^{[1
]}

Wagner, A ^{[1
]}

Mioskowski, C ^{[1
]}

机构：

[1] Univ Louis Pasteur Strasbourg 1, Lab Synthese Bioorgan, UA CNRS, F-67401 Illkirch Graffenstaden, France

来源：

TETRAHEDRON LETTERS | 1999年 / 40卷 / 05期

关键词：

esterification; nitro compounds; coupling reaction; solid-phase synthesis;

D O I：

10.1016/S0040-4039(98)02544-1

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Nitroacetic esters are prepared in good yield by reaction, at 0 degrees C, of nitroacetic acid with various alcohols in the presence of DCC, These reaction conditions were applied to the preparation of Merrifield resin-bound nitroacetate. (C) 1999 Published by Elsevier Science Ltd. All rights reserved.

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收藏

页码：875 / 878

页数：4

相关论文

共 18 条

[1] REACTIONS NITROACETIC ACID WITH ALDEHYDES AND ENAMINES [J].

ARMAREGO, WL .

JOURNAL OF THE CHEMICAL SOCIETY C-ORGANIC, 1969, (06) :986-&

[2] GAMMA-LACTAM ANALOGS OF MONOCYCLIC BETA-LACTAM ANTIBIOTICS [J].

CROSSLEY, MJ ;

CRUMBIE, RL ;

FUNG, YM ;

POTTER, JJ .

TETRAHEDRON LETTERS, 1987, 28 (25) :2883-2886

[3] ALKYL NITRATE NITRATION OF ACTIVE METHYLENE COMPOUNDS .6. NITRATION OF ESTERS IN LIQUID AMMONIA [J].

FEUER, H ;

MONTER, RP .

JOURNAL OF ORGANIC CHEMISTRY, 1969, 34 (04) :991-&

[4] UBER DEN VERLAUF DER AMINOSAURE-SYNTHESEN MIT TIRTIAREN ESTERBASEN (ZUM MECHANISMUS DER C-ALKYLIERUNGSREAKTIONEN TERTIARER MANNICH-BASEN UND QUARTARER AMMONIUMSALZE) [J].

HELLMANN, H ;

HALLMANN, G ;

LINGENS, F .

CHEMISCHE BERICHTE-RECUEIL, 1953, 86 (10) :1346-1361

[5] NEW METHOD FOR CONVERSION OF NITRO-GROUPS INTO CARBONYLS [J].

MCMURRY, JE ;

MELTON, J .

JOURNAL OF ORGANIC CHEMISTRY, 1973, 38 (26) :4367-4373

[6] NEW METHOD FOR CONVERTING NITRO-COMPOUNDS INTO CARBONYLS - OZONOLYSIS OF NITRONATES [J].

MCMURRY, JE ;

MELTON, J ;

PADGETT, H .

JOURNAL OF ORGANIC CHEMISTRY, 1974, 39 (02) :259-260

[7]

MORI H, 1984, CHEM PHARM BULL, V32, P2200

[8]

NEF JU, 1894, ANNALUSIS, V280, P264

[9]

OLAH GA, 1980, SYNTHESIS-STUTTGART, P44

[10]

Pinnick H. W., 1990, ORG REACTIONS, V38, P655, DOI DOI 10.1002/0471264180.0R038.03