A mild and efficient procedure for the conversion of aromatic carboxylic esters to secondary amides

被引：34

作者：

Arora, R ^{[1
]}

Paul, S ^{[1
]}

Gupta, R ^{[1
]}

机构：

[1] Univ Jammu, Dept Chem, Jammu 180006, India

来源：

CANADIAN JOURNAL OF CHEMISTRY | 2005年 / 83卷 / 08期

关键词：

aromatic carboxylic esters; aromatic primary amines; secondary amides; Zn dust; microwave activation;

D O I：

10.1139/V05-134

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A mild and efficient procedure has been developed for the conversion of aromatic carboxylic esters to secondary amides using reusable Zn dust with microwave heating in the presence of N,N-dimethylformamide or conventional heating by stirring in an oil bath using THF as solvent. Zn dust can be reused several times after simple washing with dil. HCl and distilled water.

引用

页码：1137 / 1140

页数：4

共 36 条

[1] An oxime-carbapalladacycle complex covalently anchored to silica as an active and reusable heterogeneous catalyst for Suzuki cross-coupling in water [J].