Photometric method for the determination of Pb2+ following separation and preconcentration using a templated ion-exchange resin

被引:35
作者
Bae, SY [1 ]
Zeng, XF [1 ]
Murray, GM [1 ]
机构
[1] Univ Maryland Baltimore Cty, Baltimore, MD 21250 USA
关键词
D O I
10.1039/a705520j
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A novel Pb2+ ion-exchange resin based on a Pb2+ ion templated polymer was used for removal and preconcentration of Pb2+ from tap and sea-water. The results from the templated resin were compared with results obtained using three other ion-exchange resins: Chelex-100, thiol-based Duolite GT-73 and a proprietary NASA polyacrylic acid resin. The ion templated resin, being most selective toward Pb2+ ions, provides a fast and virtually interference-free preconcentration procedure. The templated resin also offers an opportunity for a held-ready test kit for the determination of Pb2+ in environmental samples based on colorimetric analysis.
引用
收藏
页码:1177 / 1180
页数:4
相关论文
共 16 条
[1]  
AKIYOSHI S, 1980, ANAL CHIM ACTA, V121, P333
[2]  
BEOCKX RL, 1986, ANAL CHEM, V58, pA274
[3]   SIMULTANEOUS DETERMINATION OF 5 TRACE-METALS IN SEAWATER BY INDUCTIVELY COUPLED PLASMA ATOMIC EMISSION-SPECTROMETRY WITH ULTRASONIC NEBULIZATION [J].
BERMAN, SS ;
MCLAREN, JW ;
WILLIE, SN .
ANALYTICAL CHEMISTRY, 1980, 52 (03) :488-492
[4]  
CLARKE BL, 1959, COLORIMETRIC DETERMI, V3, P555
[5]   Waste reduction in inductively coupled plasma mass spectrometry using flow injection and a direct injection nebulizer [J].
Crain, JS ;
Kiely, JT .
JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY, 1996, 11 (07) :525-527
[6]   METAL-ION EXTRACTION WITH A THIOL HYDROPHILIC RESIN [J].
DERATANI, A ;
SEBILLE, B .
ANALYTICAL CHEMISTRY, 1981, 53 (12) :1742-1746
[7]  
FISCHER H, 1934, FRESENIUS Z ANGEW CH, V47, P90
[8]   REMOVAL OF TRACE-METALS FROM SEAWATER BY A CHELATING RESIN [J].
FLORENCE, TM ;
BATLEY, GE .
TALANTA, 1975, 22 (02) :201-204
[9]  
HILL CM, 1994, 106480 NASA
[10]   SEPARATION OF 8 TRANSITION-ELEMENTS FROM ALKALI AND ALKALINE-EARTH ELEMENTS IN ESTUARINE AND SEAWATER WITH CHELATING RESIN AND THEIR DETERMINATION BY GRAPHITE FURNACE ATOMIC-ABSORPTION SPECTROMETRY [J].
KINGSTON, HM ;
BARNES, IL ;
BRADY, TJ ;
RAINS, TC ;
CHAMP, MA .
ANALYTICAL CHEMISTRY, 1978, 50 (14) :2064-2070