Corannulene synthesis via the pyrolysis of silyl vinyl ethers

被引：41

作者：

Liu, CZ ^{[1
]}

Rabideau, PW ^{[1
]}

机构：

[1] LOUISIANA STATE UNIV,DEPT CHEM,BATON ROUGE,LA 70803

来源：

TETRAHEDRON LETTERS | 1996年 / 37卷 / 20期

关键词：

D O I：

10.1016/0040-4039(96)00588-6

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

The bis(trimethylsilyl enol ether) derived from 7,10-diacetylfluoranthene undergoes pyrolysis to afford corannulene. This is important in cases where the usual precursor, the bis(chlorovinyl) derivative, is not accessible from the diketone. Copyright (C) 1996 Elsevier Science Ltd

引用

页码：3437 / 3440

页数：4

共 21 条

[1] LOCKING THE BOWL-SHAPED GEOMETRY OF CORANNULENE - CYCLOPENTACORANNULENE
ABDOURAZAK, AH
SYGULA, A
RABIDEAU, PW
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1993, 115 (07) : 3010 - 3011
[2] BUCKYBOWLS. 2. TOWARD THE TOTAL SYNTHESIS OF BUCKMINSTERFULLERENE (C-60) - BENZ[5,6]-AS-INDACENO-[3,2,1,8,7-MNOPQR]INDENO[4,3,2,1-CDEF]CHRYSENE
ABDOURAZAK, AH
MARCINOW, Z
SYGULA, A
SYGULA, R
RABIDEAU, PW
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1995, 117 (23) : 6410 - 6411
[3] Barth W.E., 1966, J AM CHEM SOC, V88
[4] BARTH WE, 1971, J AM CHEM SOC, V93, P1730
[5] BILLUPS WE, 1993, BUCKMINSTERFULLERENE
[6] SYNTHESIS AND DYNAMICS OF THE CORANNULENE NUCLEUS
BORCHARDT, A
FUCHICELLO, A
KILWAY, KV
BALDRIDGE, KK
SIEGEL, JS
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1992, 114 (05) : 1921 - 1923
[7] HAMMOND GS, 1992, ACS S SERIES, V481
[8] HAMMOND GS, 1992, ACC CHEM RES, V25
[9] CHARGE-TRANSFER CHROMATOGRAPHY OF AROMATIC HYDROCARBONS ON THIN LAYERS AND COLUMNS
HARVEY, RG
HALONEN, M
[J]. JOURNAL OF CHROMATOGRAPHY, 1966, 25 (02): : 294 - &
[10] HIRSCH A, 1993, ANGEW CHEM INT EDIT, V32, P1138, DOI 10.1002/anie.199311381

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