Ramped-speed cross polarization MAS NMR

被引:31
作者
Samoson, A [1 ]
Tuherm, T [1 ]
Past, J [1 ]
机构
[1] NICPB, EE-12618 Tallinn, Estonia
关键词
CP; solid state NMR; MAS; fast rotation;
D O I
10.1006/jmre.2001.2302
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
The inverse cubic dependency of the acceleration of a rotor on its diameter allows for mechanical dynamics comparable to spin dynamics in coupled spin systems. Rotor acceleration up to 300 kHz/s was measured. This feature can be used to simplify existing experiments and explore entirely new ones in the study of spin topologies and material properties. (C) 2001 Academic Press.
引用
收藏
页码:264 / 267
页数:4
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