Assay of rotenone in river water by high-throughput tandem mass spectrometry and multiple-reaction monitoring methodology

被引：12

作者：

Di Donna, L ^{[1
]}

Mazzotti, F ^{[1
]}

Sindona, G ^{[1
]}

Tagarelli, A ^{[1
]}

机构：

[1] Univ Calabria, Dipartimento Chim, I-87036 Arcavacata Di Rende, CS, Italy

来源：

RAPID COMMUNICATIONS IN MASS SPECTROMETRY | 2005年 / 19卷 / 12期

关键词：

D O I：

10.1002/rcm.1953

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

The high-throughput analytical approach proposed for the assay of rotenone in lake and river waters presented here is based on atmospheric pressure chemical ionization (APCI) multiple-reaction monitoring (MRM) methodology whereby the analyte and internal standard solutions are directly analyzed, without any previous chromatographic separation. The very good accuracy is obtained by the critical choice of a reference compound that shows gas-phase chemistry similar to that of the analyte, by producing the same product ions selected for the MRM-based assay. Copyright (c) 2005 John Wiley & Sons, Ltd.

引用

页码：1575 / 1577

页数：3

共 18 条

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