Synthesis of fine particles of ZnO at 100 °C

被引:38
作者
Dhage, SR
Pasricha, R
Ravi, V [1 ]
机构
[1] Natl Chem Lab, Phys & Mat Chem Div, Pune 411008, Maharashtra, India
[2] Natl Chem Lab, Ctr Mat Characterizat, Pune 411008, Maharashtra, India
关键词
ceramics; oxides; chemical synthesis; X-ray diffraction; electron microscopy;
D O I
10.1016/j.matlet.2004.11.019
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A simple gel to crystal conversion route has been followed for the preparation of fine ZnO at 80-100 degreesC under refluxing conditions. Freshly prepared zinc hydroxide gel is allowed to crystallize under refluxing and stirring conditions for 4-6 It. Formation of fine crystallites of ZnO is confirmed by X-ray diffraction (XRD) study. Transmission electron microscope (TEM) investigations revealed that the average particle size is 100 nm for these powders. (C) 2004 Elsevier B.V All rights reserved.
引用
收藏
页码:779 / 781
页数:3
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