Growth of high quality YBCO single crystals using BaZrO3 crucibles

被引:126
作者
Liang, RX [1 ]
Bonn, DA [1 ]
Hardy, WN [1 ]
机构
[1] Univ British Columbia, Dept Phys & Astron, Vancouver, BC V6T 1Z1, Canada
来源
PHYSICA C | 1998年 / 304卷 / 1-2期
关键词
YBa2Cu3O7-x cuprate; YBCO; single crystal growth; BaZrO3; crucible; X-ray diffraction magnetization;
D O I
10.1016/S0921-4534(98)00275-5
中图分类号
O59 [应用物理学];
学科分类号
摘要
High density BaZrO3 ceramic crucibles have been successfully fabricated and used to grow high quality YBa2Cu3O7-x (YBCO) single crystals by the BaO-CuO self flux method. The ceramic crucibles are inert and insoluble in the Y2O3-BaO-CuO melt, have a long lifetime, and can be used repeatedly for crystal growth runs. The crystals grown using the crucibles have not only high chemical purity (99.99-99.995%), but also a high degree of crystalline perfection as characterized by an extremely sharp X-ray rocking curve (FWHM = 0.007 degrees), very weak magnetic flux pinning and a magnetic irreversibility line that lies about 20 K below the line for the best YSZ crucible grown crystals. (C) 1998 Published by Elsevier Science B.V. All rights reserved.
引用
收藏
页码:105 / 111
页数:7
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