Transmission electron microscopy observation of deformation microstructure under spherical indentation in silicon

被引:185
作者
Bradby, JE [1 ]
Williams, JS
Wong-Leung, J
Swain, MV
Munroe, P
机构
[1] Australian Natl Univ, Dept Elect Mat Engn, RSPhysSE, Canberra, ACT 0200, Australia
[2] Univ Sydney, Dept Mech & Mechatron Engn, Biomat Sci Res Unit, Eveleigh, NSW 1430, Australia
[3] Univ New S Wales, Electron Microscope Unit, Sydney, NSW 2052, Australia
关键词
D O I
10.1063/1.1332110
中图分类号
O59 [应用物理学];
学科分类号
摘要
Spherical indentation of crystalline silicon has been studied using cross-sectional transmission electron microscopy (XTEM). Indentation loads were chosen below and above the yield point for silicon to investigate the modes of plastic deformation. Slip planes are visible in the XTEM micrographs in both indentation loads studied. A thin layer of polycrystalline material has been identified (indexed as Si-XII from diffraction patterns) on the low-load indentation. The higher-load indentation revealed a large region of amorphous silicon. The sequence of structural deformation by indentation in silicon has been observed with the initial deformation mechanism being slip until phase transformations can take place. (C) 2000 American Institute of Physics. [S0003-6951(00)05450-4].
引用
收藏
页码:3749 / 3751
页数:3
相关论文
共 20 条
[1]   THE EXTENT OF PHASE-TRANSFORMATION IN SILICON HARDNESS INDENTATIONS [J].
CALLAHAN, DL ;
MORRIS, JC .
JOURNAL OF MATERIALS RESEARCH, 1992, 7 (07) :1614-1617
[2]   Effect of phase transformations on the shape of the unloading curve in the nanoindentation of silicon [J].
Domnich, V ;
Gogotsi, Y ;
Dub, S .
APPLIED PHYSICS LETTERS, 2000, 76 (16) :2214-2216
[3]   A SIMPLE PREDICTIVE MODEL FOR SPHERICAL INDENTATION [J].
FIELD, JS ;
SWAIN, MV .
JOURNAL OF MATERIALS RESEARCH, 1993, 8 (02) :297-306
[4]   SHEAR-INDUCED METALLIZATION [J].
GILMAN, JJ .
PHILOSOPHICAL MAGAZINE B-PHYSICS OF CONDENSED MATTER STATISTICAL MECHANICS ELECTRONIC OPTICAL AND MAGNETIC PROPERTIES, 1993, 67 (02) :207-214
[5]   Cyclic nanoindentation and Raman microspectroscopy study of phase transformations in semiconductors [J].
Gogotsi, YG ;
Domnich, V ;
Dub, SN ;
Kailer, A ;
Nickel, KG .
JOURNAL OF MATERIALS RESEARCH, 2000, 15 (04) :871-879
[6]   DEFORMATION OF SILICON AT LOW-TEMPERATURES [J].
HILL, MJ ;
ROWCLIFFE, DJ .
JOURNAL OF MATERIALS SCIENCE, 1974, 9 (10) :1569-1576
[7]   CRYSTAL DATA FOR HIGH-PRESSURE PHASES OF SILICON [J].
HU, JZ ;
MERKLE, LD ;
MENONI, CS ;
SPAIN, IL .
PHYSICAL REVIEW B, 1986, 34 (07) :4679-4684
[8]   Phase transformations of silicon caused by contact loading [J].
Kailer, A ;
Gogotsi, YG ;
Nickel, KG .
JOURNAL OF APPLIED PHYSICS, 1997, 81 (07) :3057-3063
[9]   Size-dependent phase transformations during point loading of silicon [J].
Mann, AB ;
van Heerden, D ;
Pethica, JB ;
Weihs, TP .
JOURNAL OF MATERIALS RESEARCH, 2000, 15 (08) :1754-1758
[10]   THE DEFORMATION-BEHAVIOR OF CERAMIC CRYSTALS SUBJECTED TO VERY LOW LOAD (NANO)INDENTATIONS [J].
PAGE, TF ;
OLIVER, WC ;
MCHARGUE, CJ .
JOURNAL OF MATERIALS RESEARCH, 1992, 7 (02) :450-473