Multipurpose imaging-plate camera for in-situ powder XRD at the GILDA beamline

被引:87
作者
Meneghini, C [1 ]
Artioli, G
Balerna, A
Gualtieri, AF
Norby, P
Mobilio, S
机构
[1] ESRF, GILDA, Ist Nazl Fis Mat, BP 220, F-38043 Grenoble, France
[2] Univ Rome Tre, Dip Fis E Amaldi, I-00146 Rome, Italy
[3] Univ Milan, Dipartimento Sci Terra, I-20133 Milan, Italy
[4] Ist Nazl Fis Nucl, Lab Nazl Frascati, I-00044 Frascati, Italy
[5] Univ Modena, Dipartimento Sci Terra, I-41100 Modena, Italy
[6] Univ Oslo, Dept Chem, N-0315 Oslo, Norway
关键词
imaging plate; in situ diffractometry; time-resolved;
D O I
10.1107/S090904950100992X
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
An Imaging-Plate (IP) camera for X-ray powder diffraction (XRPD) experiments was installed on the synchrotron radiation beamline GILDA at the ESRF. The IP camera can be used in fixed data-collection mode of the whole diffraction rings, or in translation mode for time-dependent experiments. The apparatus is ideal for collecting medium- to relatively high-resolution diffraction data from diluted or weakly scattering samples and to investigate in situ phase changes induced by temperature and/or chemical reactions. The possibility to rapidly collect several good quality diffraction patterns coupled with tunable beam energy allow for multiwavelength experiments such as anomalous XRPD.
引用
收藏
页码:1162 / 1166
页数:5
相关论文
共 23 条
[1]   IMAGING PLATES FOR USE WITH SYNCHROTRON-RADIATION [J].
AMEMIYA, Y .
JOURNAL OF SYNCHROTRON RADIATION, 1995, 2 :13-21
[2]   Kinetics of oxidation of fuel cell cathode materials lanthanum strontium Manganates(III)(IV) at actual working conditions:: In situ powder diffraction studies [J].
Andersen, EK ;
Andersen, IGK ;
Norby, P ;
Hanson, JC .
JOURNAL OF SOLID STATE CHEMISTRY, 1998, 141 (01) :235-240
[3]  
CANTON P, 2001, IN PRESS J CHEM PH B
[4]  
CANTON P, 2000, 0802193 GILDA ESRF
[5]   An eight-position capillary sample spinning stage for the diffractometer at BL20B at the Photon Factory [J].
Creagh, DC ;
Foran, GJ ;
Cookson, DJ ;
Garrett, RF ;
Johnson, F .
JOURNAL OF SYNCHROTRON RADIATION, 1998, 5 :823-825
[6]   POWDER DIFFRACTION USING IMAGING PLATES AT THE AUSTRALIAN NATIONAL BEAMLINE FACILITY AT THE PHOTON FACTORY [J].
GARRETT, RF ;
COOKSON, DJ ;
FORAN, GJ ;
SABINE, TM ;
KENNEDY, BJ ;
WILKINS, SW .
REVIEW OF SCIENTIFIC INSTRUMENTS, 1995, 66 (02) :1351-1353
[7]   Rietveld refinement using synchrotron X-ray powder diffraction data collected in transmission geometry using an imaging-plate detector: Application to standard m-ZrO2 [J].
Gualtieri, A ;
Norby, P ;
Hanson, J ;
Hriljac, J .
JOURNAL OF APPLIED CRYSTALLOGRAPHY, 1996, 29 (pt 6) :707-713
[8]   Development of an in-situ X-ray diffraction system for observation of electrodeposition of metallic layers [J].
Imafuku, M ;
Kurosaki, M ;
Kawasaki, K .
JOURNAL OF SYNCHROTRON RADIATION, 1998, 5 :935-936
[9]   CRYSTALLIZATION OF TETRAGONAL (B8) AND CUBIC (B1) MODIFICATIONS OF ZEOLITE NAP FROM FRESHLY PREPARED GEL .1. MECHANISM OF THE CRYSTALLIZATION [J].
KATOVIC, A ;
SUBOTIC, B ;
SMIT, I ;
DESPOTOVIC, LA .
ZEOLITES, 1989, 9 (01) :45-53
[10]  
KATOVIC A, 1989, ZEOLITES, V10, P634