A short and efficient synthesis of (±)-trans-sabinene hydrate

被引：41

作者：

Galopin, CC ^{[1
]}

机构：

[1] Givaudan Flavors Corp, Dept Res & Dev, Organ Chem Sect, Cincinnati, OH 45216 USA

来源：

TETRAHEDRON LETTERS | 2001年 / 42卷 / 33期

关键词：

D O I：

10.1016/S0040-4039(01)01081-4

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A short synthesis of sabinene hydrate is reported. It uses cheap starting materials and affordable reagents. The main product of the synthesis is trans-sabinene hydrate. (C) 2001 Elsevier Science Ltd. All rights reserved.

引用

页码：5589 / 5591

页数：3

共 20 条

[1] A convenient synthesis of trans-Sabinene hydrate from (-)-3-thujol via a highly selective ene reaction of singlet oxygen
Baeckstrom, P
Koutek, B
Saman, D
Vrkoc, J
[J]. BIOORGANIC & MEDICINAL CHEMISTRY, 1996, 4 (03) : 419 - 421
[2] Tandem lithium-ene cyclization and thiophenoxide expulsion to produce fused vinylcyclopropanes: First observation of allylic lithium oxyanion-induced reactivity and stereoselectivity in intramolecular carbolithiation
Cheng, D
Knox, KR
Cohen, T
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2000, 122 (02) : 412 - 413
[3] CONIA JM, 1968, TETRAHEDR L, V17, P2101
[4] DIMETHYLOXOSULFONIUM METHYLIDE ((CH3)2SOCH2) AND DIMETHYLSULFONIUM METHYLIDE ((CH3)2SCH2) FORMATION AND APPLICATION TO ORGANIC SYNTHESIS
COREY, EJ
CHAYKOVSKY, M
[J]. JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1965, 87 (06) : 1353 - +
[5] TOTAL SYNTHESIS OF DL-SABINENE DL-TRANS-SABINENE HYDRATE AND RELATED MONOTERPENES
FANTA, WI
ERMAN, WF
[J]. JOURNAL OF ORGANIC CHEMISTRY, 1968, 33 (04) : 1656 - &
[6] GENERATION OF TRIMETHYLSULFONIUM CATION FROM DIMETHYL-SULFOXIDE AND DIMETHYL SULFATE - IMPLICATIONS FOR THE SYNTHESIS OF EPOXIDES FROM ALDEHYDES AND KETONES
FORRESTER, J
JONES, RVH
PRESTON, PN
SIMPSON, ESC
[J]. JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1995, (18): : 2289 - 2291
[7] SYNTHESIS AND BIOLOGICAL-ACTIVITY OF NOVEL VITAMIN-D ANALOGS - 24,24-DIFLUORO-25-HYDROXY-26,27-DIMETHYLVITAMIN-D3 AND 24,24-DIFLUORO-1-ALPHA,25-DIHYDROXY-26,27-DIMETHYLVITAMIN-D3
GILL, HS
LONDOWSKI, JM
CORRADINO, RA
ZINSMEISTER, AR
KUMAR, R
[J]. JOURNAL OF MEDICINAL CHEMISTRY, 1990, 33 (02) : 480 - 490
[8] STUDIES ON CHEMICAL CONSTITUENTS OF GENUS MENTHA .2. MENTHA-CANDICANS, A NEW CHEMICAL STRAIN OF SECTION SPICATAE, CONTAINING TRANS-SABINENE HYDRATE AS PRINCIPAL COMPONENT OF ESSENTIAL OIL
KARASAWA, D
SHIMIZU, S
[J]. AGRICULTURAL AND BIOLOGICAL CHEMISTRY, 1978, 42 (02): : 433 - 437
[9] KARASAWA D, 1978, AGR BIOL CHEM TOKYO, V42, P437
[10] KUHN R, 1958, LIEBIGS ANN CHEM, V611, P117

← 1 2 →