On line extraction and separation of bendiocarb, methomyl, methylparathion, and pentachlorophenol pesticides from raw milk

被引：29

作者：

Menezes, ML

Fèlix, G

机构：

[1] Univ Estadual Paulista, Fac Ciencias, Dept Quim, BR-17033360 Bauru, SP, Brazil

[2] ENSCPB, Chim Organ & Organomet Lab, CNRS, URA 35, F-33402 Talence, France

来源：

JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES | 1998年 / 21卷 / 18期

关键词：

D O I：

10.1080/10826079808003449

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

A high performance liquid chromatography (HPLC) method for extraction and determination of pesticides from raw milk was developed. The method involves direct injection of raw milk samples on a bovine serum albumin-dimethyl-octyl-silica gel (BSA-Si-Cs) column. The mobile phase 0.05 mol.L-1 phosphate buffer pH6.0 in acetonitrile (70:30 v/v) was employed for extraction and separation of bendiocarb, methylparathion, pentachlorophenol, and methomyl pesticides. The method shows good results of recovery in the pesticides studied, higher than 99.6%.

引用

页码：2863 / 2871

页数：9

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