A high-sensitivity differential scanning calorimeter with magnetic field for magnetostructural transitions

被引：56

作者：

Marcos, J ^{[1
]}

Casanova, F ^{[1
]}

Batlle, X ^{[1
]}

Labarta, A ^{[1
]}

Planes, A ^{[1
]}

Mañosa, L ^{[1
]}

机构：

[1] Univ Barcelona, Fac Fis, E-08028 Barcelona, Catalonia, Spain

来源：

REVIEW OF SCIENTIFIC INSTRUMENTS | 2003年 / 74卷 / 11期

关键词：

D O I：

10.1063/1.1614857

中图分类号：

TH7 [仪器、仪表];

学科分类号：

0804 ; 080401 ; 081102 ;

摘要：

We have developed a differential scanning calorimeter capable of working under applied magnetic fields of up to 5 T. The calorimeter is highly sensitive and operates over the temperature range 10-300 K. It is shown that, after a proper calibration, the system enables determination of the latent heat and entropy changes in first-order solid-solid phase transitions. The system is particularly useful for investigating materials that exhibit the giant magnetocaloric effect arising from a magnetostructural phase transition. Data for Gd-5(Si0.1Ge0.9)(4) are presented. (C) 2003 American Institute of Physics.

引用

页码：4768 / 4771

页数：4

共 19 条

[1] Scaling of the entropy change at the magnetoelastic transition in Gd5(SixGe1-x)4 -: art. no. 212402 [J].

Casanova, F ;

Batlle, X ;

Labarta, A ;

Marcos, J ;

Mañosa, L ;

Planes, A .

PHYSICAL REVIEW B, 2002, 66 (21) :1-4

[2] Experimental device for studying the magnetocaloric effect in pulse magnetic fields [J].

Dankov, SY ;

Tishin, AM ;

Pecharsky, VK ;

Gschneider, KA .

REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (06) :2432-2437

[3] Comment on "Direct measurement of the 'giant' adiabatic temperature change in Gd5Si2Ge2" -: Reply [J].

Földeàki, M ;

Chahine, R ;

Bose, TK ;

Barclay, JA .

PHYSICAL REVIEW LETTERS, 2000, 85 (19) :4192-4192

[4]

GIGUERE A, 2000, PHYS REV LETT, V84, P4617

[5] MODULATED DIFFERENTIAL SCANNING CALORIMETRY [J].

GILL, PS ;

SAUERBRUNN, SR ;

READING, M .

JOURNAL OF THERMAL ANALYSIS, 1993, 40 (03) :931-939

[6] Sample translatory type insert for automated magnetocaloric effect measurements [J].

Gopal, BR ;

Chahine, R ;

Bose, TK .

REVIEW OF SCIENTIFIC INSTRUMENTS, 1997, 68 (04) :1818-1822

[7] Comment on "Direct measurement of the 'giant' adiabatic temperature change in Gd5Si2Ge2" [J].

Gschneidner, KA ;

Pecharsky, VK ;

Brück, E ;

Duijn, HGM ;

Levin, EM .

PHYSICAL REVIEW LETTERS, 2000, 85 (19) :4190-4190

[8] Nonadiabatic heat-capacity measurements using a superconducting quantum interference device magnetometer [J].

Kharkovski, AI ;

Binek, C ;

Kleemann, W .

APPLIED PHYSICS LETTERS, 2000, 77 (15) :2409-2411

[9] Modulation calorimetry and related techniques [J].

Kraftmakher, Y .

PHYSICS REPORTS-REVIEW SECTION OF PHYSICS LETTERS, 2002, 356 (1-2) :1-117

[10] Magnetic field induced entropy change and magnetoelasticity in Ni-Mn-Ga alloys -: art. no. 224413 [J].

Marcos, J ;

Planes, A ;

Mañosa, L ;

Casanova, F ;

Batlle, X ;

Labarta, A ;

Martínez, B .

PHYSICAL REVIEW B, 2002, 66 (22) :1-6

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